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首页> 外文期刊>Thermochimica Acta: An International Journal Concerned with the Broader Aspects of Thermochemistry and Its Applications to Chemical Problems >CLASSICAL TEMPERATURE-MODULATED CALORIMETRY - A REVIEW [Review]
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CLASSICAL TEMPERATURE-MODULATED CALORIMETRY - A REVIEW [Review]

机译：经典的温度调制量热法-审查[审查]

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摘要

The historical, methodological and technical development and the applications of temperature-modulated calorimetry (also known as AC calorimetry) are reviewed over the last three decades, up to about 1992. Modulation calorimetry (MC) is compared with other calorimetric methods. Particular emphasis is given to temperature scanning and frequency-dependent heat capacity experiments. Recent advances in MC, in particular the combination of differential scanning calorimetry (DSC) and modulation technique - the temperature-modulated DSC (TMDSC) - is discussed in view of measured dynamic specific heat. The theoretical models worked out before 1990 are briefly described. The Limiting boundary conditions for dynamic calorimetry are critically discussed. Some selections of experimental setups for MC, selected among about 200 citations given here, exemplify by their characteristic experimental parameters the broad variety of existing possibilities to carry out temperature-modulated calorimetric experiments. (C) 1997 Elsevier Science B.V. [References: 207]
机译：回顾了近三十年来（直到大约1992年）温度调制量热法（也称为AC量热法）的历史，方法学和技术发展以及应用。将调制量热法（MC）与其他量热法进行了比较。特别强调温度扫描和频率相关的热容实验。鉴于测量的动态比热，讨论了MC的最新进展，特别是差示扫描量热法（DSC）和调制技术-温度调制DSC（TMDSC）的结合。简要介绍了1990年前制定的理论模型。严格讨论了动态量热的极限边界条件。在这里给出的大约200个引用中，对MC的实验设置进行了一些选择，以其特有的实验参数来举例说明进行温度调制量热实验的各种现有可能性。 （C）1997 Elsevier Science B.V. [参考号：207]

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