Synthesis and crystal structure of dodecatungstic acid with icosahedron

LU Xiaoming; LIU Shuncheng; Melvyn Churchill

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Synthesis and crystal structure of dodecatungstic acid with icosahedron

机译：二十面体十二碳钨酸的合成及晶体结构

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POLYOXOMETALATES have become a unique branch in chemistry because of their application in medicine and in industry as catalyst. Furthermore, polyoxometalates pose fundamental questions with respect to the elucidation of their reactivity and general coordination chemistry, of the mechanisms of interconversion of various structural types. In our investigation of the synthesis and the catalysis of polyoxometalates, we have obtained a novel isopolytungstate of H_(16) W_(12) O_(44) centre dot 6[CH_3COCH_2COH(CH_3)_2] in which the twelve tungstate atoms constitute a type of icosahedron structure (figure 1) .

机译：聚甲醛由于在医学和工业上作为催化剂的应用已成为化学领域的独特分支。此外，多金属氧酸盐提出了关于其反应性和一般配位化学，各种结构类型的相互转化机理的基本问题。在我们对多金属氧酸盐的合成和催化的研究中，我们获得了H_（16）W_（12）O_（44）中心点6 [CH_3COCH_2COH（CH_3）_2]的新型异多钨酸盐，其中十二个钨酸盐原子构成了一个类型二十面体结构（图1）。

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《Chinese science bulletin》 |1997年第7期|共4页
作者
LU Xiaoming; LIU Shuncheng; Melvyn Churchill;
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正文语种 eng
中图分类自然科学现状及发展;
关键词
icosahedron; isopolytungstate; crystal structure;

机译：二十面体;异钨酸钨;晶体结构;

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1. Synthesis and crystal structure of dodecatungstic acid with icosahedron [J] . LU Xiaoming, LIU Shuncheng, Melvyn Churchill Chinese science bulletin . 1997,第7期

机译：二十面体十二碳钨酸的合成及晶体结构
2. Cocrystals of Penciclovir with Hydroxybenzoic Acids: Synthesis, Crystal Structures, and Physicochemical Evaluation [J] . Yuan Zhao-Jun, Dai Xia-Lin, Huang Yong-Liang, Crystal growth & design . 2020,第6期

机译：Penciclovir与羟基苯甲酸的酸咖啡：合成，晶体结构和物理化学评价
3. Synthesis and X-ray crystal structure investigations of the complexes of a proton sponge with selected inorganic acids: Crystal structure of DMAN.HI complex [J] . Lasocha W, Rafalska-Lasocha A Crystal Research and Technology: Journal of Experimental and Industrial Crystallography . 2006,第6期

机译：质子海绵与无机酸配合物的合成及X射线晶体结构研究：DMAN.HI配合物的晶体结构
4. Construction of one new coordination polymers based on 5-(pyridin-4-yl)isophthalic acid acid ligands: synthesis, crystal structures and magnetism [C] . Ya-Ning Wang, Shi-Jie Li, Wen-Dong Song International Conference on Mechatronics, Robotics and Automation . 2015

机译：基于5-（吡啶-4-基）间苯二甲酸配体的一种新配位聚合物的构建：合成，晶体结构和磁
5. I. Crystallization of CRBPII mutants as a probe for understanding wavelength regulation. II. Reengineering and crystallization of Cellular Retinol Binding Protein II (CRBPII) as a fluorescent tag. III. Synthesis of gamma-carboxy glutamic acid and applications towards the synthesis of conantokins. [D] . Watson, Camille Theonie. 2016

机译：I.CRBPII突变体的结晶作为理解波长调节的探针。二。重新设计和结晶的细胞视黄醇结合蛋白II（CRBPII）作为荧光标记。三， γ-羧基谷氨酸的合成及其在刀豆蛋白合成中的应用。
6. Synthesis and Biological Activity of Manganese (II) Complexes of Phthalic and Isophthalic Acid: X-Ray Crystal Structures of Mn(ph)(Phen)2(H2O)· 4H2O Mn(Phen)2(H2O)22(Isoph)2(Phen)· 12H2O and {Mn(Isoph)(bipy)4· 2.75biby}n(phH2 = Phthalic Acid; isoph = Isophthalic Acid; phen = 110-Phenanthroline; bipy = 22-Bipyridine) [O] . Michael Devereux, Malachy McCann, Vanessa Leon, 2000

机译：邻苯二甲酸和间苯二甲酸锰（II）配合物的合成和生物活性：Mn（ph）（Phen）2（H2O）·4H2OMn（Phen）2（H2O）2 2的X射线晶体结构（Isoph）2（Phen）·12H2O和{Mn（Isoph）（bipy） 4·2.75biby} n（phH2 =邻苯二甲酸; isoph =间苯二甲酸; phen = 110-邻菲咯啉; bipy = 22 -联吡啶）
7. Synthesis and Biological Activity of Manganese (II) Complexes of Phthalic and Isophthalic Acid: X-Ray Crystal Structures of [Mn(ph)(Phen)2(H2O)]· 4H2O, [Mn(Phen)2(H2O)2]2(Isoph)2(Phen)· 12H2O and {[Mn(Isoph)(bipy)]4· 2.75biby}n(phH2 = Phthalic Acid; isoph = Isophthalic Acid; phen = 1,10-Phenanthroline; bipy = 2,2-Bipyridine) [O] . Devereux, Michael, McCann, Malachy, Leon, Vanessa, 2000

机译：邻苯二甲酸和间苯二甲酸锰（II）配合物的合成和生物活性：[Mn（ph）（Phen）2（H2O）]·4H2O，[Mn（Phen）2（H2O）2] 2的X射线晶体结构（Isoph）2（Phen）·12H2O和{[Mn（Isoph）（bipy）] 4·2.75biby} n（phH2 =邻苯二甲酸; isoph =间苯二甲酸; phen = 1,10-邻菲咯啉; bipy = 2,2 -联吡啶）

Synthesis and crystal structure of dodecatungstic acid with icosahedron

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