~(13)C-~(13)C Chemical Shift Correlation in Rotating Solids without ~1H Decoupling During Mixing

Christian Herbst; Kerstin Riedel; Jorg Leppert

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~(13)C-~(13)C Chemical Shift Correlation in Rotating Solids without ~1H Decoupling During Mixing

机译：混合过程中没有〜1H解耦的旋转固体中〜（13）C-〜（13）C化学位移相关

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摘要

Homonuclear ~(13)C chemical shift correlation experiments are commonly employed in magic-angle spinning (MAS) solid-state NMR spectroscopy studies of biomolecular systems such as proteins and nucleic acids,both for resonance assignments and for obtaining structural constraints.

机译：Homonuclear〜（13）C化学位移相关性实验通常用于生物分子系统（例如蛋白质和核酸）的魔角旋转（MAS）固态NMR光谱研究中，既用于共振分配，也用于获得结构约束。

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《Chemphyschem: A European journal of chemical physics and physical chemistry》 |2007年第12期|共4页
作者
Christian Herbst; Kerstin Riedel; Jorg Leppert;
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正文语种 eng
中图分类物理化学（理论化学）、化学物理学;
关键词
~(13)C-~(13)C chemical shift correlation; magic-angle spinning; NMR spectroscopy; solid-state structures; transverse and longitudinal mixing;

机译：〜（13）C-〜（13）C化学位移相关;魔角旋转;NMR光谱;固态结构;横向和纵向混合;

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1. ~(13)C-~(13)C Chemical Shift Correlation in Rotating Solids without ~1H Decoupling During Mixing [J] . Christian Herbst, Kerstin Riedel, Jorg Leppert Chemphyschem: A European journal of chemical physics and physical chemistry . 2007,第12期

机译：混合过程中没有〜1H解耦的旋转固体中〜（13）C-〜（13）C化学位移相关
2. ~(13)C-~1H dipolar-driven ~(13)C-~(13)C recoupling without ~(13)C rf irradiation in nuclear magnetic resonance of rotating solids [J] . K. Takegoshi, Shinji Nakamura, Takehiko Terao The Journal of Chemical Physics . 2003,第5期

机译：〜（13）C-〜1H偶极驱动〜（13）C-〜（13）C耦合而无需〜（13）C rf辐射的旋转固体核磁共振
3. Quantitative Measurement of Transverse and Longitudinal Cross-Correlation between ~(13)C-~1H Dipolar Interaction and ~(13)C Chemical Shift Anisotropy: Application to a ~(13)C-Labeled DNA Duplex [J] . Chojiro Kojima, Akira Ono, Masatsune Kainosho, Journal of magnetic resonance . 1999,第2期

机译：〜（13）C-〜1H偶极相互作用与〜（13）C化学位移各向异性之间的横向和纵向互相关的定量测量：应用于〜（13）C标签的DNA双链体
4. FTIR and 1H MAS NMR investigations on the correlation between the frequency of stretching vibration and the chemical shift of surface OH groups of solids [C] . Eike Brunner, H.G. Karge, H.Pfeifer Univ. Leipzig Leipzig Germany. International conference on Fourier transform spectroscopy . 1992

机译：FTIR和1H MAS NMR研究关于拉伸振动频率与表面的频率与固体组的化学偏移之间的相关性
5. CRYSTAL PACKING EFFECTS ON THE PHOTOCHEMICAL OXIDATION AND SOLID STATE CARBON-13 NMR CHEMICAL SHIFTS OF SEVERAL ANTI-INFLAMMATORY STEROIDS (POLYMORPHISM, CONFORMATION, STABILITY) [D] . SUTTON, PAUL ALLEN 1984

机译：晶体包装对几种抗炎性甾体（多形，构象，稳定性）的光化学氧化和固态碳13 NMR化学位移的影响
6. Identifying Inter-Residue Resonances in Crowded 2D 13C-13C Chemical Shift Correlation Spectra of Membrane Proteins by Solid-State MAS NMR Difference Spectroscopy [O] . Yimin Miao, Timothy A. Cross, Riqiang Fu -1

机译：通过固态MAS NMR差异光谱法鉴定拥挤的2D 13C-13C膜蛋白的化学位移相关光谱中的残基间共振
7. Determination of solid-state NMR structures of proteins by means of three-dimensional 15 N– 13 C– 13 C dipolar correlation spectroscopy and chemical shift analysis [O] . Federica Castellani, Barth-jan Van Rossum, Annette Diehl, 2003

机译：通过三维15 N-13 C-13 C偶极相关光谱和化学位移分析确定蛋白质的固态NmR结构

~(13)C-~(13)C Chemical Shift Correlation in Rotating Solids without ~1H Decoupling During Mixing

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