Synthesis and characterization of a new silaborazine derivative

Cakmak H.; Jansen M.

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Synthesis and characterization of a new silaborazine derivative

机译：一种新的西拉巴嗪衍生物的合成与表征

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The synthesis and characterization of a new silaborazine derivative, namely 1,1,3,5-tetrachloro-2,6-dimethyl-4-hydride-1-silaborazine (TDSB) are reported. The monomeric TDSB molecule is structurally characterized by NMR and FT-IR spectroscopy and mass spectrometry, and additionally investigated by single crystal X-ray diffraction (P1? (No. 2); a = 7.2534(6) ?, b = 9.0788(7) ?, c = 9.1361(7) ?, α = 66.839(2)°, β = 89.348(2)°, γ = 80.502(2)° Z = 2; R1 = 0.0425 [3443 observed reflections with I > 2σ(I)]). The structure of TDSB is composed of an essentially planar SiB_2N_3 ring.

机译：报道了一种新的silaborazine衍生物，即1,1,3,5-四氯-2,6-二甲基-4-氢化物-1-silaborazine（TDSB）的合成和表征。 TDSB单体分子通过NMR，FT-IR光谱和质谱进行结构表征，并另外通过单晶X射线衍射研究（P1β（第2号）; a = 7.2534（6）β，b = 9.0788（7））？，c = 9.1361（7）？，α= 66.839（2）°，β= 89.348（2）°，γ= 80.502（2）°Z = 2; R1 = 0.0425 [3443在I>2σ（一世）]）。 TDSB的结构由基本上平面的SiB_2N_3环组成。

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《Zeitschrift fur Anorganische und Allgemeine Chemie》 |2011年第1期|共4页
作者
Cakmak H.; Jansen M.;
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正文语种 eng
中图分类化学;
关键词
Heterocycles; Si/B/N/C Ceramics; Silaborazine; Silazane cleavage; Single source precursor;

机译：杂环;Si / B / N / C陶瓷;Silaborazine;Silazane裂解;单源前体;

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Synthesis and characterization of a new silaborazine derivative

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