Solvothermal synthesis of one-dimensional chalcogenides containing group 13 elements

Ewing S.J.; Romero M.L.; Hutchinson J.; Powell A.V.; Vaqueiro P.

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Solvothermal synthesis of one-dimensional chalcogenides containing group 13 elements

机译：溶剂热合成含13族元素的一维硫族化物

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The solvothermal synthesis and characterisation of [C_6H _(16)N_2][GaS_2]_2 (1), [C _6H_(16)N_2][Ga_2Se_3(Se _2)] (2), and mixed-metal phases with composition [C_6H _(16)N_2][Ga_(2-x)In_xSe_3(Se _2)] (0 < x < 2)(3-5), is described. These materials have been characterised by single-crystal and powder X-ray diffraction, thermogravimetric analysis and UV/Vis diffuse reflectance spectroscopy. The materials contain one-dimensional anionic chains. In 1, these chains consist of edge-linked GaS_4 tetrahedra, whilst in 2-5, the chains contain perselenide (Se_2)~(2-) units and comprise alternating four-membered [M_2Se_2] and five-membered [M_2Se_3] rings (where M = Ga, In). Compounds 3-5 represent the first examples of ternary mixed-metal [M_2Se_3(Se_2)]~(2-) chains.

机译：[C_6H _（16）N_2] [GaS_2] _2（1），[C _6H_（16）N_2] [Ga_2Se_3（Se _2）]（2）和组成为[C_6H的混合金属相描述了_（16）N_2] [Ga_（2-x）In_xSe_3（Se _2）]（0

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《Zeitschrift fur Anorganische und Allgemeine Chemie》 |2012年第15期|共6页
作者
Ewing S.J.; Romero M.L.; Hutchinson J.; Powell A.V.; Vaqueiro P.;
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正文语种 eng
中图分类化学;
关键词
Chalcogens; Group 13 elements; Solid-state structures; Solvothermal synthesis; X-ray diffraction;

机译：硫族元素;13族元素;固态结构;溶剂热合成;X射线衍射;

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1. Solvothermal synthesis of one-dimensional chalcogenides containing group 13 elements [J] . Ewing S.J., Romero M.L., Hutchinson J., Zeitschrift fur Anorganische und Allgemeine Chemie . 2012,第15期

机译：溶剂热合成含13族元素的一维硫族化物
2. Synthesis of heterometallic chalcogenides containing lanthanide and group 13-15 metal elements [J] . Zhou Jian Coordination chemistry reviews . 2016,第May期

机译：含镧系元素和13-15族金属元素的杂金属硫属元素化物的合成
3. Chalcogenide/Chalcogenolate Structural Isomers of Organo Group 13 Element Derivatives: Reactions of the Dimetallenes Ar ' MMAr ' (Ar ' = C6H3-2,6-(C6H3-2,6-Pr-2(i))(2); M = Ga or In) with N2O or S-8 To Give (Ar '(ME)-E-III)(2) (E = O or S) and the Synthesis and Characterization of [Ar ' EMI](2) (M = In or Tl; E = O, S) [J] . Zhu ZL, Wright RJ, Brown ZD, Organometallics . 2009,第8期

机译：有机基团13元素衍生物的硫族化物/硫属元素化物结构异构体：双金属化合物Ar'MMAr'（Ar'= C6H3-2,6-（C6H3-2,6-Pr-2（i））（2）; M = Ga或In）与N2O或S-8生成（Ar'（ME）-E-III）（2）（E = O或S）和[Ar'EMI]（2）的合成与表征（M = In或Tl; E = O，S）
4. Controlled synthesis of one-dimensional titania nanostructure films on transparent conductive glasses from a heterogeneous solvothermal method [C] . 8th International Vacuum Electron Sources Conference and Nanocarbon . 2010

机译：异质溶剂热法控制透明导电玻璃上一维二氧化钛纳米结构薄膜的合成
5. Hydrothermal (solvothermal) and molten polychalcogenide salt synthesis of ternary and quaternary chalcogenides [D] . Liao, Ju-Hsiou 1993

机译：水热（溶剂热）和熔融多硫属元素化物盐合成三元和四元硫属元素化物
6. Multi-Element Topochemical-Molten Salt Synthesis of One-Dimensional Piezoelectric Perovskite [O] . Lihong Li, Zhongyuan Xiang, Meng Gao, 2019

机译：一维压电钙钛矿的多元素拓扑化学-熔融盐合成
7. Magnetic field-induced solvothermal synthesis of one-dimensional assemblies of Ni-Co alloy microstructures [O] . Ming Jun Hu, Bin Lin, Shu Hong Yu 2008

机译：磁场诱导的Ni-Co合金微结构一维组件的溶剂热合成
8. Minority carrier device comprising a passivating layer including a Group 13 element and a chalcogenide component [R] . 1999

机译：少数载流子器件包括钝化层，该钝化层包括第13族元素和硫族化物成分

Solvothermal synthesis of one-dimensional chalcogenides containing group 13 elements

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