One-Dimensional Channels Encapsulated in Supramolecular Networks Constructed of Zinc(II), Manganese(II), or Nickel(II) Atoms with 3-(Carboxymethyl)-2,7-dimethyl-3H-benzo[d]imidazole-5-carboxylic Acid

Mingxia Zhao; Liqin Xiong; Shilei Li; Jin Chang; Hongyu Ning; Chuanmin Qi

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One-Dimensional Channels Encapsulated in Supramolecular Networks Constructed of Zinc(II), Manganese(II), or Nickel(II) Atoms with 3-(Carboxymethyl)-2,7-dimethyl-3H-benzo[d]imidazole-5-carboxylic Acid

机译：含锌（II），锰（II）或镍（II）原子的3-（羧甲基）-2,7-二甲基-3H-苯并[d]咪唑-5-羧酸构成的超分子网络中封装的一维通道酸

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Four complexes with supramolecular architectures, namely, MZCA·3H_2O (1), [Zn(H_2O)_6]~(2+)·[MZCA]2·[H_2O]_6 (2), [Mn(MZCA)_2(H_2O)_4]·2H_2O (3), and [Ni(MZCA)_2(H_2O)_4]·2H_2O (4) [MZCA = 3-(carboxymethyl)-2,7-dimethyl-3H-benzo[d]imidazole-5-carboxylic acid], were synthesized and characterized by elemental analysis, IR spectroscopy, and single-crystal X-ray diffraction. Complexes 1 and 2 display a remarkable 3D network with 1D hydrophilic channels. Complexes 3 and 4 are isostructural and exhibit a 3D structure encapsulating 1D 24-membered ring microporous channels. The UV/Vis and fluorescent spectra were measured to characterize complexes 1-4. The thermal stability of complexes 2-4 were also examined.

机译：具有超分子结构的四个配合物，即MZCA·3H_2O（1），[Zn（H_2O）_6]〜（2+）·[MZCA] 2·[H_2O] _6（2），[Mn（MZCA）_2（H_2O） _4]·2H_2O（3）和[Ni（MZCA）_2（H_2O）_4]·2H_2O（4）[MZCA = 3-（羧甲基）-2,7-二甲基-3H-苯并[d]咪唑-5-羧酸]的合成，并通过元素分析，红外光谱和单晶X射线衍射进行表征。配合物1和2显示了具有1D亲水通道的出色3D网络。配合物3和4是同构的，并表现出3D结构，其包封1D 24元环微孔通道。测量UV / Vis和荧光光谱以表征配合物1-4。还检查了配合物2-4的热稳定性。

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来源
《Zeitschrift fur Anorganische und Allgemeine Chemie》 |2014年第1期|共9页
作者
Mingxia Zhao; Liqin Xiong; Shilei Li; Jin Chang; Hongyu Ning; Chuanmin Qi;
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正文语种 eng
中图分类化学;
关键词
Hydrogen bonding; Channels; Water chains; X-ray diffraction; Fluorescence;

机译：氢键;通道;水链;X射线衍射;荧光;

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1. One-Dimensional Channels Encapsulated in Supramolecular Networks Constructed of Zinc(II), Manganese(II), or Nickel(II) Atoms with 3-(Carboxymethyl)-2,7-dimethyl-3H-benzo[d]imidazole-5-carboxylic Acid [J] . Mingxia Zhao, Liqin Xiong, Shilei Li, Zeitschrift fur Anorganische und Allgemeine Chemie . 2014,第1期

机译：含锌（II），锰（II）或镍（II）原子的3-（羧甲基）-2,7-二甲基-3H-苯并[d]咪唑-5-羧酸构成的超分子网络中封装的一维通道酸
2. Synthesis, characterization, biological activity, molecular modeling and docking studies of complexes 4-(4-hydroxy)-3-(2-pyrazine-2-carbonyl)hydrazonomethylphenyl-diazen-yl-benzenesulfonamide with manganese(II), cobalt(II), nickel(II), zinc(II) and cadmium(II) [J] . Alaghaz Abdel-Nasser M. A., Zayed Mohamed E., Alharbi Suliman A., Journal of Molecular Structure . 2015,第Null期

机译：4-（4-羟基）-3-（2-吡嗪-2-羰基）azo嗪甲基苯基-重氮基-苯磺酰胺与锰（II），钴（II）的合成，表征，生物学活性，分子模型和对接研究，镍（II），锌（II）和镉（II）
3. A Three-Dimensional Supramolecular Network Constructed from Ti(III) Doped Doubly Bridged Molecular Ribbons catena-bis(μ-pyrazine-2,3-dicarboxylato-N,O,O')-Titanium(III)o.i5zinc(II)o.8s and Hydrated Proton via Hydrogen Bonding [J] . Xiao-Li Zhang, Ying-Zhi Zhao, Zhu Zhang Asian Journal of Chemistry: An International Quarterly Research Journal of Chemistry . 2014,第15期

机译：由Ti（III）掺杂的双桥分子带catena-bis（μ-pyrazine-2,3-dicarboxylato-N，O，O'）-Titanium（III）o.i5zinc（II）o构成的三维超分子网络.8s和通过氢键键合的水合质子
4. Liquid-Liquid Extraction of Cobalt(II), Nickel(II) and Manganese(II) from Acidic Chloride Media [C] . Alexandre Chagnes, Kateryna Omelchuk Global Conference on Extractive Metallurgy . 2018

机译：来自酸性氯化物培养基的钴（II），镍（II）和锰（II）的液液提取
5. I. Complexation of iron(II), cobalt(II), nickel(II) and copper(II) by hexadentate tripodal aminopyridyl chelators II. Binding preferences for zinc(II) relative to nickel(II) and copper(II) in novel tetradentate aminopyridyl chelators [D] . Childers, Matthew Lloyd 2007

机译：一，铁（Ⅱ），钴（Ⅱ），镍（Ⅱ）和铜（Ⅱ）与六齿三脚架氨基吡啶基螯合剂的络合作用。新型四齿氨基吡啶基螯合剂中锌（II）相对于镍（II）和铜（II）的结合偏好
6. Synthesis and Spectral Investigations of Manganese(II) Cobalt(II) Nickel(II) Copper(II) and Zinc(II) Complexes of New Polydentate Ligands Containing a 18-Naphthyridine Moiety [O] . Sreedasyam Jagannatha Swamy, Erra Ram Reddy, Devunuri Naga Raju, 2006

机译：新型含18-萘啶基多齿配体的锰（II）钴（II）镍（II）铜（II）和锌（II）配合物的合成和光谱研究
7. Differential pulse polarographic determination of nickel(II), zinc(II), cobalt(II) and manganese(II) in a 2-amino-2-methylpropanoic acid-thio-cyanate mixed system. [O] . Toru NOZAKI, Hiroshi YAMASHITA 1986

机译：在2-氨基-2-甲基丙酸 - 氰基混合系统中的差分脉冲极谱测定镍（II），锌（II），锌（II），钴（II）和锰（II）。
8. Inorganic Coordination Polymers. XXI. Manganese (II),Cobalt (II),Nickel (II),Copper (II),and Zinc (II) Bis(N-Phenylaminomethyl) Phosphinates. Effects of Coordinating Side Groups. [R] . eichelberger, j. l. gillman, h. d. 1977

机译：无机配位聚合物。 XXI。锰（II），钴（II），镍（II），铜（II）和锌（II）双（N-苯基氨基甲基）次膦酸盐。协调边群的影响。

One-Dimensional Channels Encapsulated in Supramolecular Networks Constructed of Zinc(II), Manganese(II), or Nickel(II) Atoms with 3-(Carboxymethyl)-2,7-dimethyl-3H-benzo[d]imidazole-5-carboxylic Acid

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