SYNTHESIS AND CRYSTAL STRUCTURE OF FEU8S17 [German]

Kohlmann H.; Beck HP.; Stowe K.

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SYNTHESIS AND CRYSTAL STRUCTURE OF FEU8S17 [German]

机译：FEU8S17的合成和晶体结构[德语]

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As a by-product of the synthesis of beta-US2 by chemical transport reactions black crystals of FeU8S17 were obtained, which were morphologically clearly different from the beta-US2 crystals. The composition and the crystal structure could be determined by energy dispersive X-ray fluorescence and from X-ray single crystal data. FeU8S17 crystallizes isotypically to CrU8S17 in the space group C2/m with the lattice parameters a=1334.0(3)pm, b=839.9(2)pm, c=1044.7(2) pm and beta=101.49(3)degrees (Z=2). The crystal structure and the source of the contamination with iron are discussed. [References: 14]

机译：作为通过化学转运反应合成β-US2的副产物，获得了FeU8S17黑色晶体，其形态与β-US2晶体明显不同。组成和晶体结构可以通过能量色散X射线荧光和X射线单晶数据确定。 FeU8S17在空间群C2 / m中同型结晶为CrU8S17，晶格参数为a = 1334.0（3）pm，b = 839.9（2）pm，c = 1044.7（2）pm和beta = 101.49（3）度（Z = 2）。讨论了铁的晶体结构和污染源。 [参考：14]

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《Zeitschrift fur Anorganische und Allgemeine Chemie》 |1997年第6期|共4页
作者
Kohlmann H.; Beck HP.; Stowe K.;
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正文语种 ger
中图分类化学;
关键词
Actinide chalcogenides; Iron uranium sulfides; X-ray single crystal structure determination;

机译：in系硫属元素化物;铁铀硫化物;X射线单晶结构测定;

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SYNTHESIS AND CRYSTAL STRUCTURE OF FEU8S17 [German]

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