Shape controlling synthesis - Formation of Fe3Si by the reaction of iron with silicon tetrachloride and crystal structure refinement

Schutte M.; Wartchow R.; Binnewies M.

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Shape controlling synthesis - Formation of Fe3Si by the reaction of iron with silicon tetrachloride and crystal structure refinement

机译：形状控制合成-铁与四氯化硅反应形成Fe3Si及细化晶体结构

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Pure Fe3Si is formed by the reaction of an iron-wire with SiCl4-vapor at a reaction temperature of 1000 degreesC and a SiCl4-pressure of 2 bar. Remarkable is the fact that the outer shape of the used iron wire has not been changed during the reaction. The crystal structure of Fe3Si was determined using single crystal methods. Fe3Si crystallizes in the space group Fm3m. The lattice parameters depend on the composition. [References: 7]

机译：Fe3Si是由铁丝与SiCl4蒸气在1000摄氏度的反应温度和2 bar的SiCl4压力下反应形成的。值得注意的是，反应中用过的铁丝的外形没有改变。 Fe3Si的晶体结构使用单晶方法确定。 Fe3Si在Fm3m空间群中结晶。晶格参数取决于组成。 [参考：7]

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《Zeitschrift fur Anorganische und Allgemeine Chemie》 |2003年第10期|共5页
作者
Schutte M.; Wartchow R.; Binnewies M.;
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正文语种 eng
中图分类化学;
关键词
Iron silicide; Crystal structure; Shape controlling synthesis;

机译：硅化铁;晶体结构;形状控制合成;

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1. Shape controlling synthesis - Formation of Fe3Si by the reaction of iron with silicon tetrachloride and crystal structure refinement [J] . Schutte M., Wartchow R., Binnewies M. Zeitschrift fur Anorganische und Allgemeine Chemie . 2003,第10期

机译：形状控制合成-铁与四氯化硅反应形成Fe3Si及细化晶体结构
2. Phase-Controlled Synthesis of Iron Silicide (Fe3Si and FeSi2) Nanoparticles in Solution [J] . Naween Dahal, Viktor Chikan Chemistry of Materials: A Publication of the American Chemistry Society . 2010,第9期

机译：溶液中相控合成硅化铁（Fe3Si和FeSi2）纳米粒子
3. Phase-Controlled Synthesis of Iron Silicide (Fe3Si and FeSi2) Nanoparticles in Solution [J] . Naween Dahal, Viktor Chikan Chemistry of Materials: A Publication of the American Chemistry Society . 2010,第9期

机译：溶液中相控合成硅化铁（Fe3Si和FeSi2）纳米粒子
4. Synthesis of Shape-Controlled Iron Oxide Nano-Structures in Ionic Liquids [C] . Yong Wang, Hong Yang International Symposium on Runaway Reactions, Pressure Relief Design and Effluent Handling American Institute of Chemical Engineers/American Chemical Society Management Conference . 2005

机译：离子液体中形状控制的氧化铁纳米结构的合成
5. High-index faceted Pt-based alloy nanocrystals: Shape-controlled synthesis, formation mechanisms and their structure-dependent catalytic properties. [D] . Wang, Chenyu. 2015

机译：高折射率分面铂基合金纳米晶体：形状控制的合成，形成机理及其与结构有关的催化性能。
6. Shape- size- and structure-controlled synthesis and biocompatibility of iron oxide nanoparticles for magnetic theranostics [O] . Wensheng Xie, Zhenhu Guo, Fei Gao, 2018

机译：用于磁性治疗的氧化铁纳米粒子的形状尺寸和结构受控的合成及其生物相容性
7. Formation of Metal Silicides with Silicon Tetrachloride (2nd Report). Reaction between Molybdenum and Silicon Tetrachloride [O] . Mayumi Someno, Toshimasa Aoki 1957

机译：用四氯化硅形成金属硅化物（第二次报告）。钼和四氯化硅之间的反应

Shape controlling synthesis - Formation of Fe3Si by the reaction of iron with silicon tetrachloride and crystal structure refinement

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