Crystal Structure of Ce3Ni2(BN)(2)N and magnetic behavior of (CeNi(BN))(2)(CeN)(x) with x=0, 1

Glaser J; Mori T; Meyer HJ

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Crystal Structure of Ce3Ni2(BN)(2)N and magnetic behavior of (CeNi(BN))(2)(CeN)(x) with x=0, 1

机译：Ce3Ni2（BN）（2）N的晶体结构和x = 0，1时的（CeNi（BN））（2）（CeN）（x）的磁行为

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The new compound Ce3Ni2(BN)(2)N was synthesized by a modified solid state metathesis reaction. The crystal structure of Ce3Ni2(BN)(2)N was found to be isotypic with the superconducting compound La3Ni2(BN)(2)N, according to Rietveld refinements performed on X-ray powder data (14/mmm, Z = 2, a = 3.5817(1) angstrom, c = 20.283(1) angstrom). Corresponding solid state reactions of mixtures composed of CeN/NiB and CeNi/BN yielded CeNi(BN) and a mixture of the two closely related layered structures (CeNi(BN))(2)(CeN)(x) with x = 0 and 1. Magnetization experiments on these samples revealed temperature independent paramagnetic behavior for Ce3Ni2(BN)(2)N and CeNi(BN) without any magnetic ordering down to 5 K.

机译：通过修饰的固态复分解反应合成了新的化合物Ce3Ni2（BN）（2）N。根据对X射线粉末数据进行的Rietveld改进（14 / mmm，Z = 2），发现Ce3Ni2（BN）（2）N的晶体结构与超导化合物La3Ni2（BN）（2）N同型。 a = 3.5817（1）埃，c = 20.283（1）埃）。由CeN / NiB和CeNi / BN组成的混合物的相应固相反应产生CeNi（BN）和x = 0且两个紧密相关的层状结构（CeNi（BN））（2）（CeN）（x）的混合物1.在这些样品上进行的磁化实验表明，Ce3Ni2（BN）（2）N和CeNi（BN）的温度无关顺磁行为，没有低至5 K的任何磁阶。

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《Zeitschrift fur Anorganische und Allgemeine Chemie》 |2008年第7期|共4页
作者
Glaser J; Mori T; Meyer HJ;
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正文语种 eng
中图分类化学;
关键词
nitridoborates; cerium; nickel; magnetism; BN ANIONS; SUPERCONDUCTIVITY; LA3NI2B2N3;

机译：亚硝酸硼酸盐;铈;镍;磁性;BN阴离子;超导;LA3NI2B2N3;

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Crystal Structure of Ce3Ni2(BN)(2)N and magnetic behavior of (CeNi(BN))(2)(CeN)(x) with x=0, 1

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