Synthesis of Raspberry and Ginger Ketones by Nickel Boride-catalyzed Hydrogenation of 4-Arylbut-3-en-2-ones

Mikhail Bandarenko; Vitaly Kovalenko

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Synthesis of Raspberry and Ginger Ketones by Nickel Boride-catalyzed Hydrogenation of 4-Arylbut-3-en-2-ones

机译：硼化镍催化4-芳基丁-3-烯-2-酮加氢合成树莓和姜酮

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摘要

Raspberry and ginger ketones have been synthesized in good yield by the hydrogenation of the corresponding unsaturated precursors 4-(4′-hydroxyphenyl)but-3-en-2-one and 4-(4′-hydroxy-3′-methoxyphenyl)but-3-en-2-one, respectively, using a freshly prepared suspension of nickel boride in methanol as catalyst.

机译：通过氢化相应的不饱和前体4-（4'-羟基苯基）but-3-en-2-one和4-（4'-羟基-3'-甲氧基苯基）丁酯，可以高产率合成树莓和姜酮。 -3-en-2-one分别使用新鲜制备的硼化镍在甲醇中的悬浮液作为催化剂。

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《Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences》 |2014年第8期|共4页
作者
Mikhail Bandarenko; Vitaly Kovalenko;
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原文格式 PDF
正文语种 eng
中图分类化学;
关键词
Raspberry Ketone; Zingerone; Enones; Hydrogenation; Nickel Boride;

机译：覆盆子酮;姜黄酮;烯酮;加氢;镍硼化物;

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专利

1. Synthesis of Raspberry and Ginger Ketones by Nickel Boride-catalyzed Hydrogenation of 4-Arylbut-3-en-2-ones [J] . Mikhail Bandarenko, Vitaly Kovalenko Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences . 2014,第8期

机译：硼化镍催化4-芳基丁-3-烯-2-酮加氢合成树莓和姜酮
2. Ketone Synthesis by a Nickel-Catalyzed Dehydrogenative Cross-Coupling of Primary Alcohols [J] . Verheyen Thomas, van Turnhout Lars, Vandavasi Jaya Kishore, Journal of the American Chemical Society . 2019,第17期

机译：镍催化的伯醇脱氢交叉偶联合成酮
3. Ketone Synthesis by a Nickel-Catalyzed Dehydrogenative Cross-Coupling of Primary Alcohols [J] . Verheyen Thomas, van Turnhout Lars, Vandavasi Jaya Kishore, Journal of the American Chemical Society . 2019,第17期

机译：通过镍催化的初级醇的碳催化脱氢交叉偶联的酮合成
4. Stereochemical Studies of the Enantio-differentiating Hydrogenation of Various Prochiral Ketones over Tartaric Acid-Modified Nickel Catalyst [C] . T. Sugimura, T. Osawa, S. Nakagawa International congress on catalysis;ICC . 1996

机译：酒石酸改性镍催化剂上各种手性酮的对映异构加氢的立体化学研究
5. Understanding and developing PikC as a tool in organic synthesis. Part I: Total synthesis of methymycin and neomethymycin featuring a catalytic nickel ynal cyclization and a biocatalytic PikC carbon-hydrogen oxidation. Part II: Regiodivergent nickel catalyzed macrocyclizations. [D] . Shareef, Abdur-Rafay. 2012

机译：了解和开发PikC作为有机合成工具。第一部分：甲霉素和新甲霉素的全合成，其特征在于具有催化的镍基醛环化和生物催化的PikC碳氢氧化作用。第二部分：区域发散性镍催化的大环化。
6. New phosphine-diamine and phosphine-amino-alcohol tridentate ligands for ruthenium catalysed enantioselective hydrogenation of ketones and a concise lactone synthesis enabled by asymmetric reduction of cyano-ketones [O] . José A Fuentes, Scott D Phillips, Matthew L Clarke 2012

机译：用于钌催化酮的对映选择性氢化的新膦二胺和膦氨基氨基醇三齿配体以及通过不对称还原氰基酮实现的简洁内酯合成
7. Efficient Biosynthesis of Raspberry Ketone by Engineered Escherichia coli Coexpressing Zingerone Synthase and Glucose Dehydrogenase [O] . -1

机译：通过工程化大肠杆菌共同制造覆盆子合成酶和葡萄糖脱氢酶的高效生物合成覆盆子酮

Synthesis of Raspberry and Ginger Ketones by Nickel Boride-catalyzed Hydrogenation of 4-Arylbut-3-en-2-ones

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