The first pseudo-ternary thiocyanate containing two alkali metals - synthesis and single-crystal structure of LiK2[SCN](3)

Reckeweg Olaf; DiSalvo Francis J.

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The first pseudo-ternary thiocyanate containing two alkali metals - synthesis and single-crystal structure of LiK2[SCN](3)

机译：含两种碱金属的第一种拟三元硫氰酸盐-LiK2 [SCN]（3）的合成和单晶结构

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A procedure was empirically developed to prepare the compound LiK2[SCN](3), which forms colorless, transparent, very fragile, and extremely hygroscopic thin rectangular plates. Its unique crystal structure was determined by single-crystal X-ray diffraction. LiK2[SCN](3) adopts the orthorhombic space group Pna2(1) (no. 33, Z = 4) with the cell parameters a = 1209.32(9), b = 950.85(9), and c = 849.95(6) pm.

机译：根据经验开发了一种程序来制备化合物LiK2 [SCN]（3），该化合物形成无色，透明，非常易碎且极易吸湿的矩形薄板。通过单晶X射线衍射测定其独特的晶体结构。 LiK2 [SCN]（3）采用正交结构空间群Pna2（1）（编号33，Z = 4），其单元参数为a = 1209.32（9），b = 950.85（9）和c = 849.95（6）下午。

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《Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences》 |2016年第2期|共4页
作者
Reckeweg Olaf; DiSalvo Francis J.;
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正文语种 eng
中图分类化学;
关键词
lithium; potassium; structure elucidation; thiocyanate;

机译：锂;钾;结构解析;硫氰酸盐;

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1. The first pseudo-ternary thiocyanate containing two alkali metals - synthesis and single-crystal structure of LiK2[SCN](3) [J] . Reckeweg Olaf, DiSalvo Francis J. Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences . 2016,第2期

机译：含两种碱金属的第一种拟三元硫氰酸盐-LiK2 [SCN]（3）的合成和单晶结构
2. New Family of Thiocyanate-Bridged Re(IV)-SCN-M(II) (M = Ni, Co, Fe, and Mn) Heterobimetallic Compounds: Synthesis, Crystal Structure,and Magnetic Properties [J] . Ricardo González, † Alvaro Acosta, † Raúl Chiozzone, Inorganic Chemistry . 2012,第10期

机译：硫氰酸盐桥联的Re（IV）-SCN-M（II）的新家族（M = Ni，Co，Fe和Mn）杂双金属化合物：合成，晶体结构和磁性
3. New family of thiocyanate-bridged Re(IV)-SCN-M(II) (M = Ni, Co, Fe, and Mn) heterobimetallic compounds: Synthesis, crystal structure, and magnetic properties [J] . González R., Acosta A., Chiozzone R., Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics . 2012,第10期

机译：硫氰酸盐桥联的Re（IV）-SCN-M（II）（M = Ni，Co，Fe和Mn）杂双金属化合物的新家族：合成，晶体结构和磁性
4. ELECTRONIC STRUCTURE OF THE ORGANIC METALS k-ET_2Cu(SCN)_2 AND k-ET_2CuN(CN)_2Br MEASURED BY SOFT X-RAY EMISSION AND SOFT X-RAY ABSORPTION [C] . Symposium on electrical, optical, and magnetic properties of organic solid-state materials . 1998

机译：通过软X射线发射和软X射线吸收测量的有机金属K-ET_2CU（SCN）_2和K-ET_2CU n（CN）_2 Br的电子结构
5. New alkali-metal and alkaline-earth metal borates: Synthesis, crystal structures, and optical properties [D] . Tu, Jun-Ming 1996

机译：新型碱金属和碱土金属硼酸盐：合成，晶体结构和光学性质
6. Significant Liquid-Structure Theory of Viscosity and Self-Diffusion of the Alkali Metals [O] . Chen C. Hsu, Henry Eyring 1972

机译：碱金属粘度和自扩散的重要液体结构理论
7. Understanding the Formation of New Clusters of Alkali and Alkaline Earth Metals: A New Synthetic Approach, Single-Crystal Structures, and Theoretical Calculations J. Am. Chem. Soc.2003,125, 3593−3604. [O] . Katharina M. Fromm, E. D. Gueneau, G. Bernardinelli, 2005

机译：了解碱和碱土金属新簇的形成：一种新的合成方法，单晶结构和理论计算J。是。化学。 SOC.2003,125,3593-3604。
8. Addition Compounds of Alkali Metal Hydrides. 13. Reactions of Alkali Metal Hydrides with Trialkylboranes. Synthesis and Dissociation of Alkali Metal Trialkylborohydrides. Ethyl Ether-Organoborane as a Reversible 'Solvent' for Lithium Hydride. [R] . Brown, H. C., Khuri, A., Kim, S. C. 1977

机译：碱金属氢化物的加成化合物。 13.碱金属氢化物与三烷基硼烷的反应。碱金属三烷基硼氢化物的合成与解离。乙醚 - 有机硼烷作为氢化锂的可逆“溶剂”。

The first pseudo-ternary thiocyanate containing two alkali metals - synthesis and single-crystal structure of LiK2[SCN](3)

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