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Synthesis and characterization of polypyrrole/TiO_2 composites on mild steel

机译:低碳钢上聚吡咯/ TiO_2复合材料的合成与表征

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The anodic codeposition of polypyrrole and TiO_2 on AISI 1010 steel substrates in oxalic acid medium was studied from the standpoint of their use as protective coatings against corrosion .The influence of surface treatment ,pH, stirring and current density(j) on the current efficiency(#gamma#) and pigment concentration incorporated in the polymer (C_c) were investigated.The highest C_c Values(7.5%) were found at j=5mA cm~(-2),pH 4 and stirred baths.The composites were characterized by adherence and surface roughness tesrts.XPS,EDX,SEM,FTIR and cyclic voltammetry.
机译:从草酸介质中AISI 1010钢基体上聚吡咯和TiO_2的阳极共沉积角度出发,研究了它们在防腐蚀保护层中的应用。表面处理,pH,搅拌和电流密度(j)对电流效率的影响(研究了在聚合物(C_c)中掺入的#γ#和颜料浓度。在j = 5mA cm〜(-2),pH 4和搅拌浴下,发现最高的C_c值(7.5%)。 XPS,EDX,SEM,FTIR和循环伏安法测定表面粗糙度。

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