SYNTHESES AND CHARACTERIZATION OF STARCH POLY(METHACRYLIC ACID) GRAFT COPOLYMERS

Athawale VD.; Rathi SC.

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SYNTHESES AND CHARACTERIZATION OF STARCH POLY(METHACRYLIC ACID) GRAFT COPOLYMERS

机译：淀粉（甲基丙烯酸）接枝共聚物的合成与表征

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Methacrylic acid (MA) was graft polymerized onto starch using Ce4+ initiator in aqueous medium. The dependence of grafting on the reaction variables, such as monomer and initiator concentration and time and temperature, was studied in detail. Acid hydrolysis and infrared (IR) spectroscopy were used for the confirmation of graft copolymer formation. Further, a representative graft copolymer was characterized by x-ray diffraction (XRD), thermogravimetric analysis (TGA), and differential scanning calorimetry(DSC). The solubility/swellability and the gelatinization characteristics of the copolymers are also reported. (C) 1997 John Wiley & Sons, Inc. [References: 11]

机译：使用Ce4 +引发剂在水性介质中将甲基丙烯酸（MA）接枝聚合到淀粉上。详细研究了接枝对反应变量的依赖性，例如单体和引发剂的浓度以及时间和温度。酸水解和红外（IR）光谱用于确认接枝共聚物的形成。此外，通过X射线衍射（XRD），热重分析（TGA）和差示扫描量热法（DSC）表征代表性的接枝共聚物。还报道了共聚物的溶解度/溶胀性和糊化特性。（C）1997 John Wiley＆Sons，Inc. [参考：11]

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《Journal of Applied Polymer Science》 |1997年第7期|共5页
作者
Athawale VD.; Rathi SC.;
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正文语种 eng
中图分类高分子化学（高聚物）;高分子化合物产品;有机化学;
关键词
Starch; Methacrylic acid; Grafting; Cerium; Infrared; X-ray diffraction; Thermogravimetic analysis; Differential scanning calorimetry; Methacrylic-acid; Composites;

机译：淀粉;甲基丙烯酸;接枝;铈;红外;X射线衍射;热解重量分析;差示扫描量热法;甲基丙烯酸;复合材料;

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专利

1. SYNTHESES AND CHARACTERIZATION OF STARCH POLY(METHACRYLIC ACID) GRAFT COPOLYMERS [J] . Athawale VD., Rathi SC. Journal of Applied Polymer Science . 1997,第7期

机译：淀粉（甲基丙烯酸）接枝共聚物的合成与表征
2. Syntheses and characterization of novel pH-sensitive graft copolymers of maleoylchitosan and poly(acrylic acid) [J] . Meifang Huang, Xin Jin, Yu Li, Reactive & Functional Polymers . 2006,第10期

机译：马来酰壳聚糖与聚丙烯酸的新型pH敏感接枝共聚物的合成与表征
3. Preparation of starch-poly-glutamic acid graft copolymers by microwave irradiation and the characterization of their properties [J] . Xu Jingyuan, Krietemeyer Elizabeth F., Finkenstadt Victoria L., Carbohydrate Polymers: Scientific and Technological Aspects of Industrially Important Polysaccharides . 2016,第Null期

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4. Synthesis and characterization of amphilphilic block-graft copolymers composed of poly(styrene-b-ethylene-co-propylene) and poly(methacrylic acid) by atom transfer radical polymerization [C] . Quanming Pan, Shiyong Liu, Yonghang Liu, Pacific polymer conference preprints . 1999

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5. Synthesis, complex formation, and dilute-solution associative behavior of linear poly(methacrylic acid) incorporating poly(ethylene glycol) and poly(2 -ethyl -2 -oxazoline) grafts [D] . Poe, Garrett David 2003

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6. Poly(N-isopropylacrylamide-co-2-((diethylamino)methyl)-4-formyl-6-methoxyphenyl acrylate) Environmental Functional Copolymers: Synthesis Characterizations and Grafting with Amino Acids [O] . Momen S. A. Abdelaty 2018

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7. Biodegradation of starch–graft–polystyrene and starch–graft–poly(methacrylic acid) copolymers in model river water [O] . Nikolić Vladimir, Veličković Sava, Antonović Dušan, 2013

机译：模型河水中淀粉-接枝-聚苯乙烯和淀粉-接枝-聚（甲基丙烯酸）共聚物的生物降解
8. Styrene-tert-Butyl Methacrylate and Styrene-Methacrylic Acid Block Copolymers:Synthesis and Characterization [R] . Ramireddy, C., Tuzar, Z., Prochazka, K., 1992

机译：苯乙烯 - 甲基丙烯酸叔丁酯和苯乙烯 - 甲基丙烯酸嵌段共聚物：合成和表征

SYNTHESES AND CHARACTERIZATION OF STARCH POLY(METHACRYLIC ACID) GRAFT COPOLYMERS

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