Hydrogen-bonded dimer of N, N'-(5-n-butyl-5-oxodibenzo[b, d]phosphole-3, 7-diyl)bis(benzamide) dimethylformamide solvate

Boon K. Teo; Hy Dang; Hong Zhang

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Hydrogen-bonded dimer of N, N'-(5-n-butyl-5-oxodibenzo[b, d]phosphole-3, 7-diyl)bis(benzamide) dimethylformamide solvate

机译：N，N'-（5-正丁基-5-氧二苯并[b，d]膦-3，7-二基）双（苯甲酰胺）二甲基甲酰胺溶剂化物的氢键二聚体

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摘要

The structure of a "large wing-span phosphine", in the oxide form, N, N'-(5-n-butyl-5-oxodi-benzo[b, d]phosphole-3, 7-diyl)bis(benzamide), C_(30)H_(27)N_2O_3P, cocrystallized with dimethyl-formamide (DMF), C_3H_7NO, is reported. The title compound is crystallized in a triclinic system with cell dimensions of a = 10.295(8) b = 12.743(5) c = 13.239(6) A, #alpha# = 108.14(3), #beta# = 108.16(5), #gamma# = 101.20(4) deg, and V = 1484.4(5) A~3, and forms a hydrogen-bonded dimer via two hydrogen bond linkages of the P=O...H-N type involving one of the two amide groups.

机译：N，N'-（5-正丁基-5-氧二苯并[b，d] phosphole-3，7-二基）双（苯甲酰胺）氧化物形式的“大翼展膦”的结构），报道了与二甲基甲酰胺（DMF）C_3H_7NO共结晶的C_（30）H_（27）N_2O_3P。标题化合物在三斜晶系系统中结晶，晶胞尺寸为a = 10.295（8）b = 12.743（5）c = 13.239（6）A，＃alpha＃= 108.14（3），＃beta＃= 108.16（5），＃gamma＃= 101.20（4）deg和V = 1484.4（5）A〜3，并通过P = O ... HN类型的两个氢键连接形成氢键键合的二聚体，其中涉及两个酰胺组。

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《Journal of chemical crystallography》 |1999年第3期|共4页
作者
Boon K. Teo; Hy Dang; Hong Zhang;
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正文语种 eng
中图分类晶体学;
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large wing-span phosphine; hydrogen-bonded dimer;

机译：大翼展膦;氢键二聚体;

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1. Hydrogen-bonded dimer of N, N'-(5-n-butyl-5-oxodibenzo[b, d]phosphole-3, 7-diyl)bis(benzamide) dimethylformamide solvate [J] . Boon K. Teo, Hy Dang, Hong Zhang Journal of chemical crystallography . 1999,第3期

机译：N，N'-（5-正丁基-5-氧二苯并[b，d]膦-3，7-二基）双（苯甲酰胺）二甲基甲酰胺溶剂化物的氢键二聚体
2. Crystal structure of an unknown solvate of {2,2′-[ethane-1,2-diylbis(nitrilomethanylylidene)]diphenolato-κ4O,N,N′,O′}(N-ferrocenylisonicotinamide-κN1)cobalt(II): a CoII–salen complex that forms hydrogen-bonded dimers [J] . Brautigam B., Herholdt C., Farnsworth W., Acta Crystallographica Section E: Crystallographic Communications . 2015,第9期

机译：{2,2'-[乙烷-1,2-二基双（亚硝基甲基亚甲叉基）]二酚-κ4O，N，N'，O'}（N-二茂铁基异烟酰胺-κN1）钴（II）的溶剂化物的晶体结构： CoII-salen络合物形成氢键二聚体
3. CRYSTAL STRUCTURE OF N-{(1Z)-3-OXO-1-(THIOPHEN-2-YL)-3-[(2E)-2-(THIOPHEN-2-YLMETHYLIDENE)-HYDRAZINYL]PROP-1-EN-2-YL}BENZAMIDE: N,N-DIMETHYLFORMAMIDE (1:1) SOLVATE [J] . Amit Kumar, K. N. Subbulakshmi, B. Narayana, European Chemical Bulletin . 2016,第8期

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5. Surface Dimer Engineering and Properties of GaAs(N)(Bi) Alloys [D] . Occena, Jordan M. 2018

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7. Crystal structure of an unknown solvate of {2,2′-[ethane-1,2-diylbis(nitrilomethanylylidene)]diphenolato-κ4O,N,N′,O′}(N-ferrocenylisonicotinamide-κN1)cobalt(II): a CoII–salen complex that forms hydrogen-bonded dimers [O] . Bryan Brautigam, Chelsea Herholdt, William Farnsworth, 2015

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8. New Heat-Resistant Polymer from Dimer Diamine Bismaleimide. Part 1. Preparation and Free Radical Cure of Dimer Diamine Bismaleimide [R] . DeFusco, A. A., Woodman, A. L., Martin, E. C., 1984

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Hydrogen-bonded dimer of N, N'-(5-n-butyl-5-oxodibenzo[b, d]phosphole-3, 7-diyl)bis(benzamide) dimethylformamide solvate

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