Synthesis and crystal structure of 4-(p-methoxyphenyl)-3, 5-bis(4-pyridyl)-1,2,4-triazole

Zhu DR.; Xu L.; Shao SC.; Raj SSS.; Fun HK.; You XZ.; Zhu XL.

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Synthesis and crystal structure of 4-(p-methoxyphenyl)-3, 5-bis(4-pyridyl)-1,2,4-triazole

机译：4-（对甲氧基苯基）-3，5-双（4-吡啶基）-1,2,4-三唑的合成及晶体结构

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The 4-(p-methoxyphenyl)-3,5-bis(4-pyridyl)1,2,4-triazole has been synthesized and its crystal structure has been determined by X-ray diffraction methods. It crystallizes in the monoclinic space group P2(1), with a = 12.5832(6) Angstrom, b = 7.0512(5) Angstrom, c = 18.4669(12) Angstrom, beta = 96.826(1)degrees, and D-calc = 1.345 g cm(-1) for Z = 4. In the structure, two pyridyl rings, phenyl ring, and triazole ring do not share a common plane. The most favored orientation of the pyridyl rings in the crystal is that their planes are inclined toward opposite directions with respect to the triazole ring. [References: 17]

机译：合成了4-（对甲氧基苯基）-3,5-双（4-吡啶基）1,2,4-三唑，并通过X射线衍射法测定了其晶体结构。它在单斜空间群P2（1）/ n中结晶，a = 12.5832（6）埃，b = 7.0512（5）埃，c = 18.4669（12）埃，beta = 96.826（1）度，D-对于Z = 4，calc = 1.345 g cm（-1）。在结构中，两个吡啶环，苯环和三唑环不共享同一平面。晶体中吡啶基环最优选的取向是它们的平面相对于三唑环朝相反的方向倾斜。 [参考：17]

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《Journal of chemical crystallography》 |2000年第6期|共4页
作者
Zhu DR.; Xu L.; Shao SC.; Raj SSS.; Fun HK.; You XZ.; Zhu XL.;
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正文语种 eng
中图分类晶体学;
关键词
Triazole; Crystal structure; Complexes;

机译：三唑;晶体结构;络合物;

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专利

1. Synthesis and crystal structure of 4-(p-methoxyphenyl)-3, 5-bis(4-pyridyl)-1,2,4-triazole [J] . Zhu DR., Xu L., Shao SC., Journal of chemical crystallography . 2000,第6期

机译：4-（对甲氧基苯基）-3，5-双（4-吡啶基）-1,2,4-三唑的合成及晶体结构
2. Synthesis, crystal structure and magnetic property of the novel dinuclear nickel(II) complex with 4-(p-methoxyphenyl)-3,5-bis(pyridine-2-yl)-1,2,4-triazole [J] . Jun Zhou, Jie Yang, Li Qi, Transition Metal Chemistry . 2007,第6期

机译：新型双核镍（II）与4-（对甲氧基苯基）-3,5-双（吡啶-2-基）-1,2,4-三唑的配合物的合成，晶体结构和磁性
3. Crystal and molecular structure of a novel complex [Mn(MOBPT)(H_2O)_2(NCS)_2] (MOBPT=4-(p-methoxyphenyl)-3,5-bis(pyridin-2-yl)-1,2,4-triazole) [J] . Dunru Zhu, Yan Xu, Yuhua Mei Journal of Molecular Structure . 2001,第1a3期

机译：新型配合物[Mn（MOBPT）（H_2O）_2（NCS）_2]的晶体和分子结构（MOBPT = 4-（对甲氧基苯基）-3,5-双（吡啶-2-基）-1,2， 4-三唑）
4. Synthesis, structure and thermal analysis of 3-hydrazino-4-amino-1,2,4-triazole energetic salts [C] . Jin-Ting Wu, Jian-Guo Zhang, Mou Sun, Seminar on New Trends in Research of Energetic Materials . 2013

机译：3-肼基-4-氨基-1,2,4-三唑高能盐的合成，结构和热分析
5. The Versatile Chemistry of Aryl Substituted 1,2,4-triazole Ligands in Molecular Magnetism. [D] . Savard, Didier. 2010

机译：分子磁性中芳基取代的1,2,4-三唑配体的通用化学。
6. Comparison of crystal structures of 4-(benzobthiophen-2-yl)-5-(345-trimethoxyphenyl)-2H-123-triazole and 4-(benzobthiophen-2-yl)-2-methyl-5-(345-trimethoxyphenyl)-2H-123-triazole [O] . Narsimha Reddy Penthala, Nikhil Reddy Madadi, Shobanbabu Bommagani, 2014

机译：4-（苯并b噻吩-2-基）-5-（345-三甲氧基苯基）-2H-123-三唑和4-（苯并b噻吩- 2-基）-2-甲基-5-（345-三甲氧基苯基）-2H-123-三唑
7. Synthesis and Crystal Structure of a-(2,4-Difluorophenyl)-a-(1H-1,2,4- triazole-1-ylmethyl)-1H-1,2,4-triazole-1-ethanolCu(II) Complex [O] . Yongfen Wang, Chuanzhou Bian 2014

机译：A-（2,4-二氟苯基）-A-（1H-1,2,4-三唑-1-基甲基）-1H-1,2,4-三唑-1-乙醇 Cu（ II）复合体

Synthesis and crystal structure of 4-(p-methoxyphenyl)-3, 5-bis(4-pyridyl)-1,2,4-triazole

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