L-Proline-catalysed the synthesis of aromatic aldehydes and ketones and their acridione derivatives at room temperature

Wang Fang-Ming; Bao Dan; Hu Bing-Xiang; Zhou Ze-Yu; Huang Deng-Deng; Chen Li-Zhuang; Liu Yang-Mei

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L-Proline-catalysed the synthesis of aromatic aldehydes and ketones and their acridione derivatives at room temperature

机译：L-脯氨酸在室温下催化芳香醛和酮及其and啶酮衍生物的合成

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A series of xanthene derivatives were prepared from cyclohexane-1,3-dione and aromatic aldehydes through Knoevenagel-Michael and cyclisation reactions in methanol: ethanol mixture (1:1), catalysed by a very small amount of L-proline at room temperature. Isomeric tetraketones were synthesised from dimedone and aromatic aldehydes under the same condition. Condensation of them with amines gave acridione derivatives. The crystal structure of an acridione was obtained and determined by X-ray single-crystal diffraction.

机译：在室温下，由极少量的L-脯氨酸催化，通过Knoevenagel-Michael和环化反应在甲醇：乙醇混合物（1：1）中由环己烷-1,3-二酮和芳族醛制备了一系列x吨衍生物。在相同条件下，由二甲酮和芳香醛合成了异构四酮。将它们与胺缩合得到a啶酮衍生物。获得了cri啶酮的晶体结构，并通过X射线单晶衍射确定。

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《Journal of chemical research: reviews and research papers from all branches of chemistry》 |2015年第8期|共6页
作者
Wang Fang-Ming; Bao Dan; Hu Bing-Xiang; Zhou Ze-Yu; Huang Deng-Deng; Chen Li-Zhuang; Liu Yang-Mei;
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正文语种 eng
中图分类化学;
关键词
xanthenes; tetraketones; acridone; L-proline; synthesis of aromatic aldehydes; synthesis of ketones;

机译：黄嘌呤;四酮;ac啶酮;L-脯氨酸;芳族醛的合成;酮的合成;

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1. L-Proline-catalysed the synthesis of aromatic aldehydes and ketones and their acridione derivatives at room temperature [J] . Wang Fang-Ming, Bao Dan, Hu Bing-Xiang, Journal of chemical research: reviews and research papers from all branches of chemistry . 2015,第8期

机译：L-脯氨酸在室温下催化芳香醛和酮及其and啶酮衍生物的合成
2. IS PI-BACK-BONDING IMPORTANT FOR SIGMA-BOUND ALDEHYDE AND KETONE COMPLEXES - SYNTHESIS AND STRUCTURAL CHARACTERIZATION OF AROMATIC ALDEHYDE COMPLEXES OF THE [CPFE(CO)(2)](+) CATION [J] . Cicero RL., Protasiewicz JD. Organometallics . 1995,第10期

机译：对SIGMA键合的醛和酮配合物来说是PI背胶重要的-[CPFE（CO）（2）]（+）阳离子的芳族醛配合物的合成和结构表征
3. An Expeditious and Safe Synthesis of Some Exocyclicα,β-Unsaturated Ketones by Microwave-Assisted Condensation of Cyclic Ketones with Aromatic Aldehydes over Anhydrous Potassium Carbonate [J] . RinaMondal, Tapas K.Mandal, Asok K.Mallik Organic Chemistry International . 2012,第7期

机译：无水碳酸钾微波辅助缩合环酮与芳香醛快速安全合成某些环外α，β-不饱和酮
4. Microwave-assisted synthesis of α-hydroxy aromatic ketones from α-bromo aromatic ketones [C] . Xiang Liu, Zheng-Guang Pan, Hai-Bo Chen American Institute of Chemical Engineers Annual Meeting . 2009

机译：α-溴芳香酮的微波辅助合成α-羟基芳香酮的α-羟基芳香酮
5. Part One. Synthesis of optically active tryptophan derivatives with potential activity as indoleamine 2,3-dioxygenase inhibitors: An approach via asymmetric catalytic hydrogenation. Part Two. Design, synthesis and pharmacology of selective ligands for alpha1-containing GABA(A)/benzodiazepine receptor subtypes: SAR studies of beta-carbolines at positions -3 and -6 and their corresponding bivalent ligands. Part Three. First enantiospecific total synthesis of the important biogenetic intermediates, (+)-polyneuridine and (+)-polyneuridine aldehyde, as well as 16-epi-vellosimine and macusine A. [D] . Yin, Wenyuan. 2007

机译：第一部分。具有吲哚胺2,3-二加氧酶抑制剂潜在活性的旋光色氨酸衍生物的合成：一种通过不对称催化氢化的方法。第二部分。含α1的GABA（A）/苯并二氮杂receptor受体亚型的选择性配体的设计，合成和药理作用：位于-3和-6位的β-咔啉及其相应的二价配体的SAR研究。第三部分。重要生物遗传中间体，（+）-聚神经氨酸和（+）-聚神经氨酸醛，以及16-表-维西辛和Macusine A的首次对映体全合成。
6. A convenient and eco-friendly cerium(III) chloride-catalysed synthesis of methoxime derivatives of aromatic aldehydes and ketones [O] . Iván Cortés, Teodoro S. Kaufman, Andrea B. J. Bracca 2018

机译：方便环保的氯化铈（III）催化合成芳香醛和酮的甲肟衍生物
7. On the Use of CeCl3.7H2O as a Catalyst for the Synthesis of Hydrazones Derived from Aromatic Aldehydes and Ketones [O] . Didier Farley Vargas, Brenda S. Romero, Teodoro Saul Kaufman, 2020

机译：在使用CECL3.7H2O作为合成芳族醛和酮衍生的含有丙唑的催化剂

L-Proline-catalysed the synthesis of aromatic aldehydes and ketones and their acridione derivatives at room temperature

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