Diastereoselective and one-pot synthesis of highly substituted cyclohexenones using Claisen-Schmidt condensation and Michael addition

Mousavi Mir Rasul; Gharari Hadigheh; Maghsoodlou Malek Taher; Hazeri Nourallah; Dastorani Parvaneh; Soria-Martinez Ruben; Garcia-Granda Santiago

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Diastereoselective and one-pot synthesis of highly substituted cyclohexenones using Claisen-Schmidt condensation and Michael addition

机译：使用克莱森-施密特缩合反应和迈克尔加成反应的非对映选择性和一锅法合成高度取代的环己烯酮

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A high efficient and convenient one-pot three-component diastreoselective synthesis of polysubstituted cyclohexenones in excellent yields has been developed through Michael addition and Claisen-Schmidt condensation of aldehydes and acetophenone with 3-oxo-N-phenylbutanamide using piperidine as an effective reagent under mild conditions within sort reaction time without using any previous activation.

机译：通过迈克尔加成反应以及醛和苯乙酮与3-氧代-N-苯基丁酰胺的克拉森-施密特缩合反应，开发了一种高效便捷的多取代环己烯酮的三组分二异丁烯选择性合成方法。在排序反应时间内的任何条件，而无需使用任何先前的激活。

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《Journal of chemical research: reviews and research papers from all branches of chemistry》 |2015年第9期|共6页
作者
Mousavi Mir Rasul; Gharari Hadigheh; Maghsoodlou Malek Taher; Hazeri Nourallah; Dastorani Parvaneh; Soria-Martinez Ruben; Garcia-Granda Santiago;
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正文语种 eng
中图分类化学;
关键词
highly substituted cyclohexenone; Claisen-Schmidt condensation; Michael addition; diastreoselective; multi-component reaction;

机译：高取代度的环己烯酮;Claisen-Schmidt缩合;Michael加成;非对映选择性;多组分反应;

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1. Diastereoselective and one-pot synthesis of highly substituted cyclohexenones using Claisen-Schmidt condensation and Michael addition [J] . Mousavi Mir Rasul, Gharari Hadigheh, Maghsoodlou Malek Taher, Journal of chemical research: reviews and research papers from all branches of chemistry . 2015,第9期

机译：使用克莱森-施密特缩合反应和迈克尔加成反应的非对映选择性和一锅法合成高度取代的环己烯酮
2. Diastereoselective enzymatic synthesis of highly substituted 3,4-dihydropyridin-2-ones via domino Knoevenagel condensation-Michael addition-intramolecular cyclization [J] . Liu Z.-Q., Liu B.-K., Wu Q., Tetrahedron . 2011,第50期

机译：多米诺骨牌Knoevenagel缩合-Michael加成-分子内环化的非对映选择性酶促合成高取代的3,4-二氢吡啶-2-酮
3. One-pot cascade Michael-Michael-Aldol condensation for diastereoselective synthesis of nitro-substituted cyclohexanes [J] . Yunfeng Chen, Cheng Zhong, Xiaohua Sun, Chemical Communications . 2009,第34期

机译：一锅级联Michael-Michael-Aldol缩合反应，用于非对映选择性合成硝基取代的环己烷
4. Highly efficient, one-pot, solvent-free synthesis of highly substituted imidazoles using molecular iodine as catalyst [C] . Yi-Ming Ren, Chun Cai International Conference on Chemical, Material and Metallurgical Engineering . 2012

机译：使用分子碘作为催化剂高效，单罐，无溶剂合成高度取代的咪唑
5. Cyclopropanation mediated by zinc carbenoid: The highly enantio- and diastereoselective one-pot approach [D] . Kim, Hun Young 2008

机译：类胡萝卜素锌介导的环丙烷化：高度对映和非对映选择性一锅法
6. Diastereoselective Synthesis of a Highly Substituted cis-Decahydroquinoline via a Knoevenagel Condensation [O] . Junfeng Huang, Stephen C. Bergmeier -1

机译：通过Knoevenagel缩合的非取代的顺式-十氢喹啉的非对映选择性合成
7. Diastereoselective and one-pot synthesis of highly substituted cyclohexenones using Claisen-Schmidt condensation and Michael addition [O] . Mousavi Mir Rasul, Gharari Hadigheh, Maghsoodlou Malek Taher, 2015

机译：使用Claisen-Schmidt缩合和Michael加成反应的非对映选择性和一锅法合成高度取代的环己烯酮

Diastereoselective and one-pot synthesis of highly substituted cyclohexenones using Claisen-Schmidt condensation and Michael addition

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