2-(2-Hydroxy)phenylazo derivatives of some 1,3-dicarbonyl compounds and their metal complexes

K. Krishnankutty; Muhammed Basheer Ummathur; P. Ummer

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2-(2-Hydroxy)phenylazo derivatives of some 1,3-dicarbonyl compounds and their metal complexes

机译：1,3-二羰基化合物的2-（2-羟基）苯基偶氮衍生物及其金属配合物

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2-Hydroxyphenylazo derivatives of three 1,3-dicarbonyl compounds (acetylacetone, methylacetoacetate and acetoacetanilide) have been synthesized and characterised. Analytical, IR,~1H NMR and mass spectral data indicate that the compounds exist in the intramolecularly hydrogen bonded keto-hydrazone form. Dibasic tridentate coordination of these compounds in their [M2L2] complexes (M = Ni~(II), Cu~(II) and Zn~(II)) has been established on the basis of analytical and spectral data.

机译：合成并表征了三种1,3-二羰基化合物（乙酰丙酮，乙酰乙酸甲酯和乙酰乙酰苯胺）的2-羟基苯基偶氮衍生物。分析，IR，〜1 H NMR和质谱数据表明该化合物以分子内氢键合的酮hydr形式存在。在分析和光谱数据的基础上，建立了这些化合物在其[M2L2]配合物中的二元三齿配位化合物（M = Ni〜（II），Cu〜（II）和Zn〜（II））。

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《Journal of the Indian Chemical Society》 |2010年第6期|共6页
作者
K. Krishnankutty; Muhammed Basheer Ummathur; P. Ummer;
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正文语种 eng
中图分类化学;
关键词
2-Hydroxyphenylazo derivatives; phenyl hydrazones; keto-hydrazone; metal complexes;

机译：2-羟基苯偶氮衍生物;苯hydr;酮hydr;金属配合物;

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1. 2-(2-Hydroxy)phenylazo derivatives of some 1,3-dicarbonyl compounds and their metal complexes [J] . K. Krishnankutty, Muhammed Basheer Ummathur, P. Ummer Journal of the Indian Chemical Society . 2010,第6期

机译：1,3-二羰基化合物的2-（2-羟基）苯基偶氮衍生物及其金属配合物
2. Synthesis of 1,2,3,5-tetrasubstituted pyrrole derivatives from 2-(2-bromoallyl)-1,3-dicarbonyl compounds [J] . Demir AS., Akhmedov DM., Sesenoglu O. Tetrahedron . 2002,第49期

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机译：环金属化反应。 IX。 2-（苯基偶氮）苯基铱（III）的配合物。

2-(2-Hydroxy)phenylazo derivatives of some 1,3-dicarbonyl compounds and their metal complexes

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