Thin layer chromatography of amino acids on impregnated and unimpregnated silica gel layers developed with water-in-oil microemulsion

Ali Mohammad; Shahna Anwar; Vineeta Agrawal

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Thin layer chromatography of amino acids on impregnated and unimpregnated silica gel layers developed with water-in-oil microemulsion

机译：油包水型微乳液开发的浸渍和未浸渍硅胶层上氨基酸的薄层色谱法

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Thin layer chromatographic behavior of twentyfour amino acids has been examined on plain silica gel as well as silica gel layers impregnated with cationic and anionic aqueous solutions using water-in-oil microemulsion as mobile phase. The impregnated plates were stable and gave well-formed spots. Silica gel impregnated with 2% CuSO_4 solution was found most suitable layer material for selective separation of DL-phenylalanine from other amino acids. The limit of detection of some amino acids has also been determined.

机译：使用油包水型微乳液作为流动相，已经在普通硅胶以及用阳离子和阴离子水溶液浸渍的硅胶层上检查了二十四个氨基酸的薄层色谱行为。浸渍的板是稳定的，并形成了良好的斑点。发现用2％CuSO 4溶液浸渍的硅胶是最合适的层材料，用于从其他氨基酸中选择性分离DL-苯丙氨酸。还确定了某些氨基酸的检出限。

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《Journal of the Indian Chemical Society》 |1999年第9期|共4页
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Ali Mohammad; Shahna Anwar; Vineeta Agrawal;
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正文语种 eng
中图分类化学;
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1. Thin layer chromatography of amino acids on impregnated and unimpregnated silica gel layers developed with water-in-oil microemulsion [J] . Ali Mohammad, Shahna Anwar, Vineeta Agrawal Journal of the Indian Chemical Society . 1999,第9期

机译：油包水型微乳液开发的浸渍和未浸渍硅胶层上氨基酸的薄层色谱法
2. Reversed phase thin layer chromatography of amino acids on silicone fluid DC200,triaryl phosphate and tri-n-butylamine impregnated silica gel-G layers [J] . S.D.Sharma, H.Sharma, C.Sharma Journal of the Indian Chemical Society . 2003,第10期

机译：硅胶流体DC200，磷酸三芳基酯和三正丁胺浸渍的硅胶G层上氨基酸的反相薄层色谱法
3. Resolution and isolation of enantiomers of (+/-)-isoxsuprine using thin silica gel layers impregnated with L-glutamic acid, comparison of separation of its diastereomers prepared with chiral derivatizing reagents having L-amino acids as chiral auxiliaries [J] . Bhushan Ravi, Nagar Hariom Biomedical Chromatography: An International Journal Devoted to Research in Chromatographic Methodologies and Their Applications in the Biosciences . 2015,第3期

机译：使用浸有L-谷氨酸的薄硅胶层拆分和分离（+/-）-异苏氨酸的对映异构体，比较用以L-氨基酸为手性助剂的手性衍生试剂制备的非对映异构体的分离
4. Application of a mixture of Oxidized Multi-walled Carbon Nanotubes and D-(-)-tartaric Acid-impregnated Silica Gel as Stationary Phases for Thin-layer Chromatographic Enantioseparation [C] . Zhi Guang Peng, Dong Hong Yin, Jian Fu Liu, International Conference on Materials and Products Manufacturing Technology . 2013

机译：将氧化多壁碳纳米管和D - （ - ） - 酒酸浸渍硅胶混合物的施用在薄层色谱肾上腺素映射分析中的固定相
5. Water-in-oil microemulsions: Counterion effects in AOT systems and new fluorocarbon-based microemulsion gels. [D] . Pan, Xiaoming. 2010

机译：油包水型微乳液：AOT系统和新型碳氟化合物微乳液凝胶中的抗衡离子效应。
6. The fractionation of phosphatidylinositol into molecular species by thin-layer chromatography on silver nitrate-impregnated silica gel [O] . 1972

机译：硝酸银浸渍硅胶上的薄层色谱法将磷脂酰肌醇分馏为分子种类
7. The fractionation of phosphatidylinositol into molecular species by thin-layer chromatography on silver nitrate-impregnated silica gel [O] . Luthra, M. G., Sheltawy, A. 1972

机译：硝酸银浸渍硅胶上的薄层色谱法将磷脂酰肌醇分馏为分子种类

Thin layer chromatography of amino acids on impregnated and unimpregnated silica gel layers developed with water-in-oil microemulsion

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