In situ generation and intramolecular schmidt reaction of keto azides in a microwave-assisted flow format

Painter T.O.; Thornton P.D.; Orestano M.; Santini C.; Organ M.G.; Aubé J.

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In situ generation and intramolecular schmidt reaction of keto azides in a microwave-assisted flow format

机译：微波辅助流动形式的叠氮化酮的原位生成和分子内施密特反应

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摘要

Go with the flow! A method for conversion of keto halides to lactams by means of sequential azidation and intramolecular Schmidt reaction in a combined flow format is described (see scheme; MWI=microwave irradiation, TFA=trifluoroacetic acid).

机译：顺其自然！描述了一种通过顺序叠氮化和分子内Schmidt反应以组合流动形式将酮卤化物转化为内酰胺的方法（参见方案; MWI =微波辐射，TFA =三氟乙酸）。

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《Chemistry: A European journal》 |2011年第35期|共4页
作者
Painter T.O.; Thornton P.D.; Orestano M.; Santini C.; Organ M.G.; Aubé J.;
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正文语种 eng
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continuous flow; keto azides; lactams; microwave chemistry; Schmidt reaction;

机译：连续流动;叠氮化物;内酰胺;微波化学;施密特反应;

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专利

1. In Situ Generation and Intramolecular Schmidt Reaction of Keto Azides in a Microwave-Assisted Flow Format [J] . Dr. Thomas O. Painter, Dr. Paul D. Thornton, Mario Orestano, Chemistry - A European Journal . 2011,第35期

机译：微波辅助流动形式下叠氮化酮的原位生成和分子内施密特反应
2. Intramolecular and intermolecular Schmidt reactions of alkyl azides with aldehydes [J] . Huey-Lih Lee, Jeffrey Aube Tetrahedron . 2007,第36期

机译：烷基叠氮化物与醛的分子内和分子间Schmidt反应
3. INTRAMOLECULAR SCHMIDT REACTIONS OF ALKYL AZIDES WITH KETALS AND ENOL ETHERS [J] . Mossman CJ., Aube J. Tetrahedron . 1996,第10期

机译：烷基和烯醇醚与烷基叠氮化物的分子内SCHMIDT反应
4. Generation of In-Situ Proppant through Hydro-Thermal Reactions [C] . Songyang Tong, Chammi Miller, and Kishore Mohanty SPE Hydraulic Fracturing Technology Conference and Exhibition . 2019

机译：通过水力热反应产生原位支撑剂
5. A Combined Allylic Azide Rearrangement and Intramolecular Schmidt Reaction -- Discovery, Development, and Application. [D] . Liu, Ruzhang. 2012

机译：烯丙基叠氮化物重排和分子内Schmidt反应的结合-发现，开发和应用。
6. In Situ Generation and Intramolecular Schmidt Reaction of Keto Azides in a Microwave-Assisted Flow Format [O] . Thomas O. Painter, Paul D. Thornton, Mario Orestano, -1

机译：在微波辅助流动形式中酮滤氮的原位代和分子内施密特反应
7. Intramolecular Schmidt Reaction of Alkyl Azides with Pentafluorophenyl Esters [O] . Zhiqi Cao, Rui Li, Yan Su, 2020

机译：烷基叠氮化烷烃与五氟苯基酯的分子内施胶反应

In situ generation and intramolecular schmidt reaction of keto azides in a microwave-assisted flow format

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