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Quantitative in situ TEM tensile testing of an individual nickel nanowire

机译:单个镍纳米线的定量原位TEM拉伸测试

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摘要

In this paper, we have demonstrated the usage of a novel micro-mechanical device (MMD) to perform quantitative in situ tensile tests on individual metallic nanowires inside a transmission electron microscope (TEM). Our preliminary experiment on a 360nm diameter nickel nanowire showed that the sample fractured at an engineering stress of ~ 1.2GPa and an engineering strain of ~ 4%, which is consistent with earlier experiments performed inside a scanning electron microscope (SEM). With in situ high resolution TEM imaging and diffraction capabilities, this novel experimental set-up could provide unique opportunities to reveal the underlying deformation and damage mechanisms for metals at the nanoscale.
机译:在本文中,我们演示了使用新型微机械装置(MMD)对透射电子显微镜(TEM)内的各个金属纳米线进行定量原位拉伸测试的方法。我们在直径为360nm的镍纳米线上进行的初步实验表明,样品在〜1.2GPa的工程应力和〜4%的工程应变下断裂,这与早期在扫描电子显微镜(SEM)中进行的实验一致。借助原位高分辨率TEM成像和衍射功能,这种新颖的实验装置可以提供独特的机会来揭示纳米级金属的潜在变形和破坏机理。

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