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Fabrication and characterization of Zn_(1-x)Al_xO nanoparticles by DC arc plasma

机译:直流电弧等离子体制备并表征Zn_(1-x)Al_xO纳米粒子

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摘要

In this paper we have introduced a simple method for the fabrication of aluminum doped zinc oxide (AZO) nanoparticles. The Zn_(1-x)Al _xO nanoparticles with different concentrations of Al (x=0.01, 0.03, 0.06, 0.09, 0.12) were fabricated successfully by this method. The samples were analyzed by the use of several techniques such as SEM, EDX, XRD, PL and UVvis spectroscopy. The SEM images showed that the fabricated nanoparticles had spherical shapes. The XRD patterns of the samples indicated that the Al atoms substituted in the Zn positions in the crystal lattice of ZnO and there were some changes in the lattice parameters. A blue shift in the λ _(max) of the absorption and a red shift in the λ_(max) of the emission were observed. The results also indicated that the amount of shifts had a direct relationship with the changes in the lattice parameters.
机译:在本文中,我们介绍了一种简单的制造铝掺杂氧化锌(AZO)纳米粒子的方法。通过该方法成功地制备了不同浓度的Al(x = 0.01、0.03、0.06、0.09、0.12)的Zn_(1-x)Al_xO纳米粒子。通过使用多种技术(例如SEM,EDX,XRD,PL和UVvis光谱法)分析样品。 SEM图像显示所制备的纳米颗粒具有球形形状。样品的X射线衍射图谱表明,Al原子取代了ZnO晶格中Zn位置,晶格参数发生了一些变化。观察到吸收的λ_(max)发生蓝移,并且发射的λ_(max)发生红移。结果还表明,偏移量与晶格参数的变化有直接关系。

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