Synthesis and structure of Zr(IV)- and Ce(IV)-based CAU-24 with 1,2,4,5-tetrakis(4-carboxypheny)benzene

Lammert M.; Reinsch H.; Murray C. A.; Wharmby M. T.; Terraschke H.; Stock N.

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Synthesis and structure of Zr(IV)- and Ce(IV)-based CAU-24 with 1,2,4,5-tetrakis(4-carboxypheny)benzene

机译：含1,2,4,5-四（4-羧基苯）苯的Zr（IV）和Ce（IV）基CAU-24的合成和结构

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Two new MOFs denoted as M-CAU-24 (M = Zr, Ce) based on 1,2,4,5-tetrakis(4-carboxyphenyl)benzene (H4TCPB) were obtained under mild reaction conditions within 15 min. The MOFs with composition [M-6(mu(3)-O)(4)(mu(3)-OH)(4)(OH)(4)(H2O)(4)(TCPB)(2)] crystallise in the scu topology, a connectivity hitherto unreported for Zr-MOFs with tetracarboxylate linker molecules. Zr-CAU-24 exhibits UV/blue ligand-based luminescence.

机译：在15分钟内在温和的反应条件下获得了基于1,2,4,5-四（4-羧基苯基）苯（H4TCPB）的两个新的MOF，称为M-CAU-24（M = Zr，Ce）。组成为[M-6（mu（3）-O）（4）（mu（3）-OH）（4）（OH）（4）（H2O）（4）（TCPB）（2）的MOF结晶在scu拓扑中，迄今为止尚未报道具有四羧酸盐连接分子的Zr-MOF的连接性。 Zr-CAU-24表现出基于UV /蓝配体的发光。

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《Dalton transactions: An international journal of inorganic chemistry》 |2016年第47期|共5页
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Lammert M.; Reinsch H.; Murray C. A.; Wharmby M. T.; Terraschke H.; Stock N.;
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机译：含1,2,4,5-四（4-羧基苯）苯的Zr（IV）和Ce（IV）基CAU-24的合成和结构
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7. Synthesis and structure of Zr(iv)- and Ce(iv)-based CAU-24 with 1,2,4,5-tetrakis(4-carboxyphenyl)benzene [O] . M. Lammert, H. Reinsch, C. A. Murray, 2016

机译：Zr（iv）和Ce（iv）的合成与结构 - 基于1,2,4,5-四苯基（4-羧基苯基）苯的Cau-24

Synthesis and structure of Zr(IV)- and Ce(IV)-based CAU-24 with 1,2,4,5-tetrakis(4-carboxypheny)benzene

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