Studies on poly(8-hydroxy-4-azoquinolinephenylmethacrylate) and its metal complexes

Vijayalakshmi S; Subramanian S; Rajagopan S; Kaliyappan T

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Studies on poly(8-hydroxy-4-azoquinolinephenylmethacrylate) and its metal complexes

机译：聚（8-羟基-4-偶氮喹啉甲基丙烯酸苯酯）及其金属配合物的研究

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8-Hydroxy-4-azoquinolinephenylmethacrylate (8H4AQPMA) was prepared and polymerized in ethyl methyl ketone (EMK) at 65 degrees C using benzoyl peroxide as free radical initiator. Poly(8-hydroxy-4-azoquinolinephenylmethacrylate) poly(8H4AQPMA) was characterized by infrared and nuclear magnetic resonance techniques. The molecular weight of the polymer was determined by gel permeation chromatography. Cu(II) and Ni(II) complexes of poly(8H4AQPMA) were prepared. Elemental analysis of polychelates suggests that the metal-ligand ratio is about 1:2. The polychelates were further characterized by infrared spectra, X-ray diffraction, spectral studies, and magnetic moments. Thermal analyses of the polymer and polychelates were carried out in air. (c) 2005 Wiley Periodicals, Inc.

机译：制备8-羟基-4-偶氮喹啉甲基丙烯酸苯酯（8H4AQPMA），并在65摄氏度下使用过氧化苯甲酰作为自由基引发剂在乙基甲基酮（EMK）中进行聚合。采用红外和核磁共振技术对聚（8-羟基-4-偶氮喹啉苯基甲基丙烯酸酯）聚（8H4AQPMA）进行了表征。通过凝胶渗透色谱法测定聚合物的分子量。制备了聚（8H4AQPMA）的Cu（II）和Ni（II）配合物。聚螯合物的元素分析表明，金属-配体比率约为1：2。通过红外光谱，X射线衍射，光谱研究和磁矩进一步表征了多螯合物。聚合物和聚螯合物的热分析在空气中进行。（c）2005年Wiley Periodicals，Inc.

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《Journal of Applied Polymer Science》 |2006年第4期|共7页
作者
Vijayalakshmi S; Subramanian S; Rajagopan S; Kaliyappan T;
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正文语种 eng
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ion exchangers; metal-polymer complexes; radical polymerization; SCHIFF-BASE; POLYMERS; SPECTRA; AMINE; IONS;

机译：离子交换剂;金属-聚合物配合物;自由基聚合;SCHIFF-BASE;聚合物;SPECTRA;胺;离子;

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Studies on poly(8-hydroxy-4-azoquinolinephenylmethacrylate) and its metal complexes

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