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Nanoscratch testing to assess the fiber adhesion of short-carbon-fiber composites

机译:纳米划痕测试,以评估短碳纤维复合材料的纤维粘附性

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In a composite material, the degree of adhesion between the fiber and the matrix plays an important role in the overall performance of the material. Because the load between the fiber and the matrix is realized throughout the interphase region material, a lot of effort has gone into characterizing the strength of the interphase. In this study, nanoscratch tests on the composite samples were used to provide a relative measure of adhesion in different composite materials. Carbon-filled nylon 6,6 and polycarbonate resins were evaluated with this method. The carbon fillers we used were polyacrylonitrile-based carbon fibers sized and surface-treated for the respective matrix and pitch-based carbon fibers without any sizing or surface treatment. Tensile and X-ray photoelectron spectroscopy data for the composites we considered are also presented to compare to the nanoscratch results. It is shown that nanoscratch testing on the composites, with the proposed data analysis, can be an effective tool for determining the relative degree of adhesion between different composites. (C) 2006 Wiley Periodicals, Inc. J Appl Polyrn Sci 103: 328-335, 2007
机译:在复合材料中,纤维与基体之间的粘合程度在材料的整体性能中起着重要作用。由于在整个相间区域材料中都实现了纤维和基体之间的负载,因此在表征相间强度方面付出了很多努力。在这项研究中,对复合材料样品的纳米划痕测试用于提供不同复合材料的粘附力的相对测量。用这种方法评估了碳填充尼龙6,6和聚碳酸酯树脂。我们使用的碳填料是聚丙烯腈基碳纤维,其尺寸和表面处理分别针对基质和沥青基碳纤维,没有任何上浆或表面处理。我们还考虑了复合材料的拉伸和X射线光电子能谱数据,以与纳米划痕结果进行比较。结果表明,采用建议的数据分析方法,对复合材料进行纳米划痕测试可以有效地确定不同复合材料之间的相对粘合程度。 (C)2006 Wiley Periodicals,Inc. J Appl Polyrn Sci 103:328-335,2007年

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