Different morphologies of the dry physical gels as a function of the sample preparation method

Pyzalska M.; Smal M.; Luboradzki R.

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Different morphologies of the dry physical gels as a function of the sample preparation method

机译：干燥物理凝胶的不同形态随样品制备方法的变化

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Xerogels obtained by drying the gels formed by glucofuranose derivatives with organic solvents were studied. The xerogels were characterized using the SEM, XRD, DSC and OPM techniques. The morphology of a xerogel observed by SEM may change from 'amorphous, fibrillar' to 'crystal-like', which may be caused by time or temperature. The results suggest that a similar transition may take place when the xerogel is being prepared. Thus SEM pictures of xerogels should be treated with great caution as they may not reflect the gelator network morphology in the bulk gel.

机译：研究了通过用有机溶剂干燥葡萄糖呋喃糖衍生物形成的凝胶而获得的干凝胶。使用SEM，XRD，DSC和OPM技术对干凝胶进行了表征。 SEM观察到的干凝胶形态可能会从“无定形，原纤维”变为“晶体状”，这可能是由时间或温度引起的。结果表明，制备干凝胶时可能发生类似的转变。因此，干凝胶的SEM图片应格外小心，因为它们可能无法反映散装凝胶中的凝胶网络形态。

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《Journal of Non-Crystalline Solids: A Journal Devoted to Oxide, Halide, Chalcogenide and Metallic Glasses, Amorphous Semiconductors, Non-Crystalline Films, Glass-Ceramics and Glassy Composites》 |2011年第17期|共6页
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Pyzalska M.; Smal M.; Luboradzki R.;
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正文语种 eng
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关键词
Gel; LMOG; Phase transition; SEM; Xerogel;

机译：凝胶;LMOG;相变;SEM;干凝胶;

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1. Different morphologies of the dry physical gels as a function of the sample preparation method [J] . Pyzalska M., Smal M., Luboradzki R. Journal of Non-Crystalline Solids: A Journal Devoted to Oxide, Halide, Chalcogenide and Metallic Glasses, Amorphous Semiconductors, Non-Crystalline Films, Glass-Ceramics and Glassy Composites . 2011,第16a17期

机译：干燥物理凝胶的不同形态随样品制备方法的变化
2. Gel-aided sample preparation (GASP)-A simplified method for gel-assisted proteomic sample generation from protein extracts and intact cells [J] . Fischer Roman, Kessler Benedikt M. Proteomics . 2015,第7期

机译：凝胶辅助样品制备（GASP）-从蛋白质提取物和完整细胞生成凝胶辅助蛋白质组样品的简化方法
3. Development of microwave-assisted drying methods for sample preparation for dried spot micro-X-ray fluorescence analysis [J] . Link DD., Kingston HM., Havrilla GJ., Analytical chemistry . 2002,第5期

机译：微波辅助干燥方法的制备，用于干点微X射线荧光分析的样品制备
4. QUANTIFICATION OF GALLIUM IN DRIED RESIDUE SAMPLES BY XRF: AN IMPROVED SAMPLE PREPARATION METHOD FOR ANALYZING PLUTONIUM METAL [C] . Christopher G. Worley Annual conference on applications of X-ray analysis . 2002

机译：XRF的干燥残余物样品中镓的定量：改进的分析钚金属样品制备方法
5. A study of the physical and chemical stability of spray dried aluminum hydroxycarbonate and of drying methods for aluminum hydroxycarbonate gel: Part I. The physical and chemical stability of spray dried aluminum hydroxycarbonate gel. Part II. Drying methods for aluminum hydroxycarbonate gel. [D] . Hancock, Kim Elaine. 1994

机译：喷雾干燥的羟基碳酸铝的物理和化学稳定性及其干燥方法的研究：第一部分。喷雾干燥的羟基碳酸铝的物理和化学稳定性。第二部分羟基碳酸铝凝胶的干燥方法。
6. Gel-aided sample preparation (GASP)—A simplified method for gel-assisted proteomic sample generation from protein extracts and intact cells [O] . Roman Fischer, Benedikt M Kessler -1

机译：凝胶辅助样品制备（GASP）-一种从蛋白质提取物和完整细胞生成凝胶辅助蛋白质组样品的简化方法
7. Gel-aided sample preparation (GASP) - a simplified method for gel-assisted proteomic sample generation from protein extracts and intact cells [O] . Fischer, R, Kessler, BM 2015

机译：凝胶辅助样品制备（GASP）-一种从蛋白质提取物和完整细胞生成凝胶辅助蛋白质组样品的简化方法
8. Quantification of gallium in dried residue samples by xrf: an improved samplepreparation method for analyzing plutonium metal [R] . Worley, C. G. 2001

机译：通过xrf定量干燥残留物样品中的镓：用于分析钚金属的改进的样品制备方法

Different morphologies of the dry physical gels as a function of the sample preparation method

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