Copper-catalyzed C-S direct cross-coupling of thiols with 5-arylpenta-2,4-dienoic acid ethyl ester

Cai Rongrong; Zhou Zhuoda; Chai Qianqian; Zhu Yueer; Xu Runsheng

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Copper-catalyzed C-S direct cross-coupling of thiols with 5-arylpenta-2,4-dienoic acid ethyl ester

机译：用5-芳基 - 2,4-二烯酸乙酯的硫醇的铜催化的C-S直接交叉偶联

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摘要

A selective copper (Cu)-catalyzed C-S bond direct cross-coupling of thiols with 5-arylpenta-2,4-dienoic acid ethyl ester was developed. Notably, various biologically active 5-phenyl-3-phenylsulfanylpenta-2,4-dienoic acid ethyl ester derivatives were efficiently synthesized under moderate conditions. Finally, a plausible Cu(I)/Cu(III) reaction mechanism was proposed.

机译：开发了一种选择性铜（Cu） - 用5-芳基 - 2,4-己二烯酸乙酯的催化C-S键直接交叉偶联。值得注意的是，在中等条件下有效地合成各种生物活性5-苯基-3-苯基磺酰戊基-2,4-二烯酸乙酯衍生物。最后，提出了一种合理的Cu（I）/ Cu（III）反应机理。

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《RSC Advances》 |2018年第47期|共9页
作者
Cai Rongrong; Zhou Zhuoda; Chai Qianqian; Zhu Yueer; Xu Runsheng;
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作者单位

Zhejiang A&

F Univ Jiyang Coll Dept Biol &

Environm Shaoxing 311800 Zhejiang Peoples R China;

Zhejiang A&

F Univ Jiyang Coll Dept Biol &

Environm Shaoxing 311800 Zhejiang Peoples R China;

Zhejiang A&

F Univ Jiyang Coll Dept Biol &

Environm Shaoxing 311800 Zhejiang Peoples R China;

Zhejiang A&

F Univ Jiyang Coll Dept Biol &

Environm Shaoxing 311800 Zhejiang Peoples R China;

Zhejiang A&

F Univ Jiyang Coll Dept Biol &

Environm Shaoxing 311800 Zhejiang Peoples R China;

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正文语种 eng
中图分类化学;
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1. Copper-catalyzed C-S direct cross-coupling of thiols with 5-arylpenta-2,4-dienoic acid ethyl ester [J] . Cai Rongrong, Zhou Zhuoda, Chai Qianqian, RSC Advances . 2018,第47期

机译：用5-芳基 - 2,4-二烯酸乙酯的硫醇的铜催化的C-S直接交叉偶联
2. Efficient copper-catalyzed C-S cross-coupling of heterocyclic thiols with aryl iodides [J] . Niu L.-F., Cai Y., Liang C., Tetrahedron . 2011,第16期

机译：铜催化杂环硫醇与芳基碘化物的C-S交叉偶联
3. Stereodefined and polyunsaturated inhibitors of histone deacetylase based on (2E,4E)-5-arylpenta-2,4-dienoic acid hydroxyamides. [J] . Marson CM, Serradji N, Rioja AS, Bioorganic and Medicinal Chemistry Letters . 2004,第10期

机译：基于（2E，4E）-5-芳基戊-2,4-二烯酸羟酰胺的组蛋白脱乙酰基酶的立体定义和多不饱和抑制剂。
4. Direct Detection of Fatty Acid Ethyl Esters using Low Temperature Plasma (LTP) Ambient Ionization Mass Spectrometry for Rapid Bacterial Differentiation [C] . J. Isabella Zhang, Anthony B. Costa, W. Andy Tao, American Society for Mass Spectrometry Conference on Mass Spectrometry and Allied Topics . 2011

机译：使用低温等离子体（LTP）环境电离质谱法直接检测脂肪酸乙酯，用于快速细菌分化
5. Copper-catalyzed cross-coupling reactions of organotrifluoroborate salts and organoboronic acids: Formation of enol esters and sulfones [D] . Huang, Fang 2007

机译：铜催化的有机三氟硼酸盐和有机硼酸的交叉偶联反应：烯醇酯和砜的形成
6. Stereocontrolled Synthesis of α-Amino-α′-alkoxy Ketones by a Copper-Catalyzed Cross-Coupling of Peptidic Thiol Esters and α-Alkoxyalkylstannanes [O] . Hao Li, Anyu He, John R. Falck, -1

机译：的立体控制合成α氨基α - 烷氧基酮通过肽类硫醇酯的铜 - 催化的交叉偶联和α-alkoxyalkylstannanes
7. Copper-catalyzed C–S direct cross-coupling of thiols with 5-arylpenta-2,4-dienoic acid ethyl ester [O] . Rongrong Cai, Zhuoda Zhou, Qianqian Chai, 2018

机译：用5-芳基 - 2,4-二烯酸乙酯的硫醇的铜催化的C-S直接交叉偶联
8. Fatty Acid Ethyl Esters of Rhizopus Arrhizus. Ethyl Esters of Long-Chain Fatty Acids Are Reported for Rhizopus Arrhizus [R] . Laseter, J. L., Weete, J. D. 1970

机译：Rhizopus arrhizus的脂肪酸乙酯。 Rhizopus arrhizus报道了长链脂肪酸的乙酯

Copper-catalyzed C-S direct cross-coupling of thiols with 5-arylpenta-2,4-dienoic acid ethyl ester

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