Rieche formylation of carbon nanotubes - one-step and versatile functionalization route

Kolanowska Anna; Kuziel Anna; Li Yuliu; Jurczyk Sebastian; Boncel Slawomir

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Rieche formylation of carbon nanotubes - one-step and versatile functionalization route

机译：碳纳米管的Rieche甲型丁二保区 - 一步和多功能官能化途径

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We present the direct and one-step Rieche formylation of carbon nanotubes (CNTs) as the most effective (4.00 mmol g(-1)) functionalization route via formylation. Indeed, classical methods, i.e. three-step protocols based on CNT oxidation-reduction-partial oxidation (COOH CH2OH CHO), were revealed as less effective and more troublesome. All CNT-CHO products were comprehensively analysed by cross-verified potentiometric titration, scanning electron microscopy (SEM), thermogravimetry (TGA), Fourier transform infrared spectroscopy (FT-IR) and Raman spectroscopy.

机译：我们将碳纳米管（CNT）的直接和一步式Rieche丁二保区作为最有效的（4.00mmol G（-1））官能化途径通过甲型化。实际上，古典方法，即基于CNT氧化还原部分氧化的三步方案（COOH CH 2 OH CHO），被揭示为较低有效和更麻烦。通过交叉验证的电位滴定，扫描电子显微镜（SEM），热重转（TGA），傅里叶变换红外光谱（FT-IR）和拉曼光谱，全面分析所有CNT-CHO产品。

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《RSC Advances》 |2017年第81期|共8页
作者
Kolanowska Anna; Kuziel Anna; Li Yuliu; Jurczyk Sebastian; Boncel Slawomir;
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作者单位

Silesian Tech Univ Dept Organ Chem Bioorgan Chem &

Biotechnol Krzywoustego 4 PL-44100 Gliwice Poland;

Silesian Tech Univ Dept Organ Chem Bioorgan Chem &

Biotechnol Krzywoustego 4 PL-44100 Gliwice Poland;

Silesian Tech Univ Dept Organ Chem Bioorgan Chem &

Biotechnol Krzywoustego 4 PL-44100 Gliwice Poland;

Inst Engn Polymer Mat &

Dyes Sklodowskiej Curie 55 PL-87100 Torun Poland;

Silesian Tech Univ Dept Organ Chem Bioorgan Chem &

Biotechnol Krzywoustego 4 PL-44100 Gliwice Poland;

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正文语种 eng
中图分类化学;
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1. Rieche formylation of carbon nanotubes - one-step and versatile functionalization route [J] . Kolanowska Anna, Kuziel Anna, Li Yuliu, RSC Advances . 2017,第81期

机译：碳纳米管的Rieche甲型丁二保区 - 一步和多功能官能化途径
2. One-Step Route Synthesized Co2P/Ru/N-Doped Carbon Nanotube Hybrids as Bifunctional Electrocatalysts for High-Performance Li-O_2 Batteries [J] . Peng Wang, Caixia Li, Shihua Dong, Small . 2019,第30期

机译：一步路线合成CO2P / RU / N掺杂的碳纳米管杂交物作为高性能Li-O_2电池的双官能电催化剂
3. A one-step route to solubilised, purified or functionalised single-walled carbon nanotubes [J] . Clancy A. J., Melbourne J., Shaffer M. S. P. Journal of Materials Chemistry, A. Materials for energy and sustainability . 2015,第32期

机译：一步一步制备，纯化或功能化的单壁碳纳米管的途径
4. One-Step Synthesizing Functionalized Multi-walled Carbon Nanotubes by Free-Radical Modification and the Application for Fuel Cells [C] . Shu-Hang LIAO, Chuan-Yu YEN, Chih-Hung HUNG Asian-Australasian Association for Composite Materials Meeting . 2008

机译：单步合成官能化多壁碳纳米管通过自由基改性和燃料电池的应用
5. Dissolution, processing and fluid structure of graphene and carbon nanotube in superacids: The route toward high performance multifunctional materials [D] . Behabtu, Natnael. 2012

机译：石墨烯和碳纳米管在超强酸中的溶解，加工和流体结构：通往高性能多功能材料的途径
6. Evaluating the biological risk of functionalized multiwalled carbon nanotubes and functionalized oxygen-doped multiwalled carbon nanotubes as possible toxic carcinogenic and embryotoxic agents [O] . Luis A Lara-Martínez, Felipe Massó, Eduardo Palacios González, 2017

机译：评估功能化的多壁碳纳米管和功能化的氧掺杂的多壁碳纳米管作为可能的有毒致癌和胚胎毒性试剂的生物风险
7. A one-step route to solubilised, purified or functionalised single-walled carbon nanotubes [O] . Clancy AJ, Melbourne J, Shaffer MSP 2015

机译：溶解，纯化或功能化的单壁碳纳米管的一步法

Rieche formylation of carbon nanotubes - one-step and versatile functionalization route

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