Analytical study of modern paint layers on metal knight shields: The use and effect of Titanium white

Clara Bratt Lauridsen; Jana Sanyova; Kim Pilkj?r Simonsen

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Analytical study of modern paint layers on metal knight shields: The use and effect of Titanium white

机译：金属骑士盾牌现代涂料层的分析研究：钛白钛的使用与效果

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Painted metal knight shields of the Order of the Elephant produced during the last part of the 20th century are characterized by a striking variety in their conservation state. Three different coat systems were identified and investigated by Fourier transform infrared microscopy (μ-FTIR), micro-Raman spectroscopy (MRS), scanning electron microscopy-Energy dispersive X-ray spectroscopy (SEM-EDX) and Thermally assisted hydrolysis and methylation-gas chromatography-mass Spectrometry (THM-GC-MS). Chalking of the white paint layer on the first group of knight shields displayed in the window niches was found to be related to the use of titanium white of the anatase type. A pristine condition of the second group could be attributed to priming of the lead rich metal support with a zinc potassium chromate based primer and the use of mainly stable white pigments in the top coat. Severe delamination of the paint layer of the third group was caused by the formation of lead corrosion products between the paint layer and the metal support. The results are discussed in relation to the climatic conditions as well as the historical context of contemporary paint production and availability in Denmark.

机译：20世纪的最后一部分在20世纪的最后一部分产生的大象顺序的被绘制的金属骑士盾牌的特征在于他们的保护状态醒目。通过傅立叶变换红外显微镜（μ-FTIR），微拉曼光谱（MRS），扫描电子显微镜 - 能量分散X射线光谱（SEM-EDX）和热辅助水解和甲基化 - 气体研究了三种不同的涂层系统。色谱 - 质谱（THM-GC-MS）。发现在窗口中显示的第一组骑士屏蔽上的白色涂料层被发现与锐钛矿类型的钛白色的使用有关。第二组的原始状况可归因于富含富金属载体的引发与基于磷酸锌的磷酸锌的底漆，并且主要在顶层中使用主要稳定的白色颜料。第三组的涂料层的严重分层是由涂料层和金属载体之间的引线腐蚀产物形成引起的。结果是关于气候条件的讨论以及当代油漆生产和丹麦可用性的历史背景。

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《Spectrochimica acta, Part A. Molecular and biomolecular spectroscopy》 |2014年第null期|共8页
作者
Clara Bratt Lauridsen; Jana Sanyova; Kim Pilkj?r Simonsen;
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作者单位

School of Conservation Esplanaden 34 DK-1263 Copenhagen K Denmark;

Laboratories of IRPA/KIK Parc du Cinquantenaire 1 1000 Brussels Belgium;

School of Conservation Esplanaden 34 DK-1263 Copenhagen K Denmark;

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正文语种 eng
中图分类光化学分析法（光谱分析法）;
关键词
Titanium white; Modern paint; Paint on metal; Raman; FTIR; THM-GC-MS;

机译：钛白色;现代涂料;金属上的涂料;拉曼;FTIR;THM-GC-MS;

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1. Analytical study of modern paint layers on metal knight shields: The use and effect of Titanium white [J] . Clara Bratt Lauridsen, Jana Sanyova, Kim Pilkj?r Simonsen Spectrochimica acta, Part A. Molecular and biomolecular spectroscopy . 2014,第Null期

机译：金属骑士盾牌现代涂料层的分析研究：钛白钛的使用与效果
2. Multi-analytical non-invasive study of modern yellow paints from postwar Italian paintings from the International Gallery of Modern Art Ca Pesaro, Venice [J] . Izzo Francesca Caterina, Capogrosso Valentina, Gironda Michele, X-Ray Spectrometry: An International Journal . 2015,第4期

机译：战后意大利威尼斯国际现代美术馆Ca Pesaro画廊的意大利绘画现代黄色颜料的多分析非侵入性研究
3. Multi-analytical Study of the Paint Layers Used in Authentication of Icon from XIXth Century [J] . Cristache Raluca Anamaria, Sandu Irina Crina Anca, Simionescu Atena Elena, Revista de Chimie . 2015,第7期

机译：十九世纪用于图标认证的油漆层的多分析研究
4. SEM and XEDS Analysis of Paint Layers on a 1907 Model G White Steam Touring Car from The Henry Ford Museum Collection [C] . Steven King, Clara Deck, Cathy Selvius DeRoo, International Metallographic Society Annual meeting;Microscopy Society of America Annual Meeting;Microanalysis Society Annual meeting . 2011

机译：亨利·福特博物馆收藏的1907年G型白色蒸汽房车上的漆层的SEM和XEDS分析
5. Electrical and materials characterization of tungsten-titanium diffusion barrier layers and alloyed silver metallization. [D] . Bhagat, Shekhar Kumar. 2008

机译：钨钛扩散阻挡层和合金化银金属的电气和材料表征。
6. Titanium dioxide: environmental white knight? [O] . L Frazer 2001

机译：二氧化钛：环保白骑士？
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8. Experimental Study to Determine a Technique for Loading Reproducible Mud Layers on Urethane-Painted Metal Surfaces [R] . Lopez, J. D. 1987

机译：确定聚氨酯涂漆金属表面可再生泥层加载技术的实验研究

Analytical study of modern paint layers on metal knight shields: The use and effect of Titanium white

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