Cp_2TiCl-catalyzed, concise synthetic approach to marine natural product (±)-cyclozonarone

Antonio Rosales Martínez; Laura Pozo Morales; Emilio Díaz Ojeda

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Cp_2TiCl-catalyzed, concise synthetic approach to marine natural product (±)-cyclozonarone

机译：CP_2TICL催化，简化习惯性的海洋天然产物（±）-cyclozonarone

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摘要

A concise synthetic approach to the bioactive marine natural product (±)-cyclozonarone has been reported from readily available epoxy-farnesol acetate. Key steps of this protocol include Cp_2TiCl-catalyzed radical cascade cyclization of an epoxy-farnesol derivative and a Diels-Alder reaction between a 1,3-diene and p-benzoquinone.

机译：从易于使用的环氧树脂 - 法内酚乙酸盐报道了生物活性海鲜天然产物（±）环酮的简明综合方法。该方案的关键步骤包括环氧树脂衍生物的CP_2TICL催化的自由基级联环化和1,3-二烯和对苯醌之间的DIEL-桤木反应。

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来源
《Synthetic Communications》 |2019年第20期|共7页
作者
Antonio Rosales Martínez; Laura Pozo Morales; Emilio Díaz Ojeda;
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作者单位

Department of Chemical Engineering University of Sevilla Sevilla Spain;

Department of Chemical Engineering University of Sevilla Sevilla Spain;

Department of Chemical Engineering University of Sevilla Sevilla Spain;

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原文格式 PDF
正文语种 eng
中图分类有机化学;
关键词
Cyclozonarone; diastereoselective synthesis; green chemistry; natural products; radical chemistry; titanocene;

机译：环状基因;非对映选择性合成;绿色化学;天然产品;激进化学;二本官;

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1. Cp_2TiCl-catalyzed, concise synthetic approach to marine natural product (±)-cyclozonarone [J] . Antonio Rosales Martínez, Laura Pozo Morales, Emilio Díaz Ojeda Synthetic Communications . 2019,第17a20期

机译：CP_2TICL催化，简化习惯性的海洋天然产物（±）-cyclozonarone
2. A Concise and Rapid Approach to the Marine Natural Product Streptochlorin and its Analogues [J] . Hee Jae Shin, Hyi-Seung Lee, Jong Seok Lee, Bulletin of the Korean Chemical Society . 2013,第2期

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3. A new approach to the C_(28) fatty acid chain of the marine natural products schulzeines B and C: A concise diastereoselective total synthesis of(-)-schulzeine B [J] . Yang C., Bao Y.-H., Liang P., Tetrahedron . 2011,第34期

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4. Search for Marine Natural Products Facilitating Astrocyte Differentiation [C] . Wai Lam Tse, Yoichi Nakao 日本化学会春季年会 . 2020

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5. Synthetic Studies Toward Marine Natural Product Okadaic Acid and Its Analogs. [D] . Fang, Chao. 2011

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6. Genome Mining and Synthetic Biology in Marine Natural Product Discovery [O] . Maria Costantini 2020

机译：基因组矿业和综合生物在海洋自然产品发现中
7. Concise Total Synthesis of the Marine Natural Product Ageladine A [O] . -1

机译：简化船舶天然产物的总合成Ageladine a
8. Chemical and Physical Properties and Thermal Decomposition Products of Certain Natural Products and Synthetic Materials [R] . Melvin, W. W. 1972

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Cp_2TiCl-catalyzed, concise synthetic approach to marine natural product (±)-cyclozonarone

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