Synthesis of novel bis- and poly(aryldiazenylthiazoles)

Mostafa E. Salem; Mohamed Hosny; Ahmed F. Darweesh; Ahmed H. M. Elwahy

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Synthesis of novel bis- and poly(aryldiazenylthiazoles)

机译：新型双和聚（芳基亚丁噻唑）的合成

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摘要

A novel series of bis- and poly(arydiazenyl)thiazoles were prepared in good yields by the reaction of the appropriate a-keto-hydrazonoyl chlorides with the corresponding bis- and poly(hydrazinecarbothioamide) in refluxing EtOH/DMF in the presence of few drops of TEA. Based on elemental analyses as well as spectral data, the structures of the new compounds were confirmed.

机译：通过在几滴存在下反转EtOH / DMF的相应双和聚（HONDAZINARBOTHIOME），通过对应的双 - 和聚（肼（HydazinaRbothiOmide）的反应，以良好的产率制备一种新的双和聚（芳亚苯基）噻唑。在几滴存在下回流EtOH / DMF 茶。基于元素分析以及光谱数据，确认了新化合物的结构。

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来源
《Synthetic Communications》 |2019年第20期|共11页
作者
Mostafa E. Salem; Mohamed Hosny; Ahmed F. Darweesh; Ahmed H. M. Elwahy;
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作者单位

Chemistry Department Faculty of Science Cairo University Giza Egypt;

Chemistry Department Faculty of Science Cairo University Giza Egypt;

Chemistry Department Faculty of Science Cairo University Giza Egypt;

Chemistry Department Faculty of Science Cairo University Giza Egypt;

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原文格式 PDF
正文语种 eng
中图分类有机化学;
关键词
Bis(arydiazenyl)thiazoles; poly(arydiazenyl)thiazoles; α-keto-hydrazonoyl chlorides; bis(thiosemicarbazones); poly(thiosemicarbazones);

机译：双唑（阿里二亚苯基）噻唑？聚（芳亚二苯基）噻唑;A-酮 - 肼酰氯;BIS（硫代蓟司障人）;聚（硫代虫虫草）;

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1. Synthesis of novel bis- and poly(aryldiazenylthiazoles) [J] . Mostafa E. Salem, Mohamed Hosny, Ahmed F. Darweesh, Synthetic Communications . 2019,第17a20期

机译：新型双和聚（芳基亚丁噻唑）的合成
2. Synthesis, photochemical, and electrochemical properties of naphthalene-1,4,5,8-tetracarboxylic acid-bis-(N,N'-bis-(2,2,4(2,4,4)-trimethylhexylpolyimide)) and poly(N,N'-bis-(2,2,4(2,4,4)-trimethyl-6-aminohexyl) 3,4,9,10-perylenetetracarboxdiimide) [J] . Yuney K, Icil H European Polymer Journal . 2007,第6期

机译：萘-1,4,5,8-四羧酸-双-（N，N'-双-（2,2,4（2,4,4）-三甲基己基聚酰亚胺））的合成，光化学和电化学性质（N，N'-双-（2,2,4（2,4,4）-三甲基-6-氨基己基）3,4,9,10-per四羧二酰亚胺）
3. Synthesis, characterization and electrical properties of poly[bis-(2-aminophenyl)disulfide] and poly[bis(2-aminophenyl)diselenide] [J] . F. R. Diaz, C. O. Sanchez Synthetic Metals . 1999,第3期

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4. Improved Synthesis and Corrosion Properties of Poly(bis-(dialkylamino)phenylene vinylene)s (BAMPPV) [C] . Nicole Anderson, David J. Irvin, Jennifer A. Irvin, Symposium on Electroactive Polymers for Corrosion Control, Dec, 2000, Sweden . 2000

机译：聚（双-（二烷基氨基）亚苯基亚乙烯基）（BAMPPV）的合成与腐蚀性能的改进
5. Expanding the Redox Chemistry of Yttrium, the Lanthanides, and Uranium through Synthesis and Reactivity of Bis-, Tris-, and Tetrakis-(Trimethylsilylcyclopentadienyl) Complexes. [D] . MacDonald, Matthew R. 2013

机译：通过Bis-，Tris-和Tetrakis-（三甲基甲硅烷基环戊二烯基）配合物的合成和反应性，扩大钇，镧系元素和铀的氧化还原化学。
6. A Facile Solvent Free Claisen-Schmidt Reaction: Synthesis of αα′-bis-(Substituted-benzylidene)cycloalkanones and αα′-bis-(Substituted-alkylidene)cycloalkanones [O] . A. F. M. Motiur Rahman, Roushown Ali, Yurngdong Jahng, 2012

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7. catena-Poly[[{bis-[tetra-aqua-(2-hy-droxy-3,4-dioxocyclo-but-1-en-1-olato-κO)bariumstrontium(0.35/0.65)]di-μ-aqua}-bis-(μ-2-hy-droxy-4-oxocyclo-but-1-ene-1,3-diolato-κO:O)] monohydrate]. [O] . Trifa, Chahrazed, Bouhali, Amira, Bouacida, Sofiane, 2011

机译：阳离子多聚[[{双-[四-水-（2-羟基--3,4-二氧代环-丁-1-烯-1-醇-κO）钡锶（0.35 / 0.65）]di-μ-水}-双-（μ-2-羟基-4-氧代环丁-1-烯-1,3-二醇基-κO：O）]一水合物]。
8. Synthesis of Bis-(Trifluoromethyl) Trisulfide and Bis-(Trifluoromethylthio)Selenide [R] . Munavalli, S., Rossman, D. I., Rohrbaugh, D. K., 1992

机译：双（三氟甲基）三硫化物和双 - （三氟甲硫基）硒化物的合成

Synthesis of novel bis- and poly(aryldiazenylthiazoles)

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