Tetrazolyl and dinitromethyl groups with 1,2,3-triazole lead to polyazole energetic materials

Liu Yingle; He Chunlin; Tang Yongxing; Imler Gregory H.; Parrish Damon A.; Shreeve Jeanne M.

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Tetrazolyl and dinitromethyl groups with 1,2,3-triazole lead to polyazole energetic materials

机译：具有1,2,3-三唑的四唑和二硝基甲基导致聚唑能量材料

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A class of polyazole energetic compounds (combination of tetrazolyl, dinitromethyl and triazole) was obtained from 4,5-dicyanotriazole. All the new compounds were fully characterized by IR, NMR [H-1, C-13 {H-1}], elemental analysis, and differential scanning calorimetry (DSC). Compounds 5, 6 and 8 were further characterized with single-crystal X-ray diffraction studies. Heats of formation and detonation performances were determined using Gaussian 03 and EXPLO5 v6.01 programs, which show that 5 is a promising green primary explosive and 7 as a secondary explosive has a detonation velocity superior to 1,3,5-trinitro-triazacyclohexane (RDX).

机译：一类聚唑能量化合物（四唑基，二硝基甲基和三唑）的组合从4,5-二氰基唑得到。所有新化合物通过IR，NMR [H-1，C-13 {H-1}，元素分析和差示扫描量热法（DSC）完全表征。通过单晶X射线衍射研究进一步表征化合物5,6和8。使用高斯03和爆炸性测定形成和爆炸性能的热量，并利用5 v6.01节目，表明5是有前景的绿色初级炸药，7作为二次爆炸性的爆炸速度优于1,3,5-三腈 - 三氮杂环己烷（ RDX）。

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《Dalton transactions: An international journal of inorganic chemistry》 |2019年第10期|共6页
作者
Liu Yingle; He Chunlin; Tang Yongxing; Imler Gregory H.; Parrish Damon A.; Shreeve Jeanne M.;
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Sichuan Univ Sci &

Engn Sch Chem &

Environm Engn 180 Xueyuan St Zigong 643000 Sichuan Peoples R China;

Beijing Inst Technol Sch Mat Sci &

Engn 5 South Zhongguancun St Beijing 100081 Peoples R China;

Univ Idaho Dept Chem Moscow ID 83844 USA;

Naval Res Lab Code 6910 4555 Overlook Ave Washington DC 20375 USA;

Naval Res Lab Code 6910 4555 Overlook Ave Washington DC 20375 USA;

Univ Idaho Dept Chem Moscow ID 83844 USA;

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正文语种 eng
中图分类化学;无机化学;
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1. Tetrazolyl and dinitromethyl groups with 1,2,3-triazole lead to polyazole energetic materials [J] . Liu Yingle, He Chunlin, Tang Yongxing, Dalton transactions: An international journal of inorganic chemistry . 2019,第10期

机译：具有1,2,3-三唑的四唑和二硝基甲基导致聚唑能量材料
2. A Safer Synthesis of 3,5-Bis(dinitromethyl)-1,2,4-triazole (BDT) and Its Mono and Di Salts: High-Performance Insensitive Energetic Materials [J] . Dharavath Srinivas, Shreeve Jeanne M. Propellants, Explosives, Pyrotechnics . 2018,第1期

机译：3,5-双（二硝基甲基）-1,2,4-三唑（BDT）及其单盐和二盐的更安全合成：高性能不敏感的能量材料
3. Nitramino-and Dinitromethyl-Substituted 1,2,4-Triazole Derivatives as High-Performance Energetic Materials [J] . Yongxing Tang, Srinivas Dharavath, Gregory H. Imler, Chemistry: A European journal . 2017,第38期

机译：硝基氨基和二硝基甲基取代的1,2,4-三唑衍生物作为高性能能量材料
4. Synthesis of a new energetic metal-organic framework based on Gem-dinitromethyl substituted 1,2,3-triazole [C] . Hao Gu, Qing Ma, Guangbin Cheng, Seminar on new trends in research of energetic materials . 2019

机译：基于Gem-二硝基甲基取代的1,2,3-三唑的新型高能金属有机骨架的合成
5. New Thermally Stable Materials: I. Nucleophilic Azoles with Cyclic Perfluoroalkenes: II. Trifluoromethyl or Pentafluorosulfanyl Substituted Poly-1,2,3-triazoles; and III. Silver and Copper Derivatives of FOX-7 [D] . Garg, Sonali 2010

机译：新的热稳定材料：I.带有环状全氟烯烃的亲核腈：II。用三氟甲基或五氟硫烷基取代的聚1,2,3-三唑;和III。 FOX-7的银和铜衍生物
6. Synthesis and Properties of Energetic Hydrazinium5-Nitro-3-dinitromethyl-2H-pyrazoleby Unexpected Isomerization of N-Nitropyrazole [O] . Yiying Zhang, Yanan Li, Tao Yu, 2019

机译：高能Hy的合成及性质5-硝基-3-二硝基甲基-2H-吡唑-N-硝基噻唑的意外异构化反应
7. Cover Feature: Gem -dinitromethyl-substituted Energetic Metal-Organic Framework based on 1,2,3-Triazole from in situ Controllable Synthesis (Chem. Asian J. 19/2018) [O] . Hao Gu, Qing Ma, Shiliang Huang, 2018

机译：封面特点：基于1,2,3-三唑的珠宝硝基甲基取代的能量金属 - 有机框架，原位可控合成（Chem.亚洲J.19/2018）
8. Synthesis, Characterization, and Structural Investigations of 1-amino-3-Substituted- 1,2,3-Triazolium Salts, and a New Route to 1-substituted-1,2,3- triazoles [R] . Kaplan, G. , Drake, G. , Tollison, K. , 2004

机译：1-氨基-3-取代-1,2,3-三唑盐的合成，表征和结构研究，以及1-取代-1,2,3-三唑的新途径

Tetrazolyl and dinitromethyl groups with 1,2,3-triazole lead to polyazole energetic materials

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