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首页> 外文期刊>Journal of Applied Polymer Science >A novel approach for synthesis of poly(norbornene)‐ coco ‐poly(styrene) block copolymers via metathesis polymerization and free‐radical polymerization
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A novel approach for synthesis of poly(norbornene)‐ coco ‐poly(styrene) block copolymers via metathesis polymerization and free‐radical polymerization

机译：一种用于合成聚（降冰片烯）的新方法 - co Co -poly（苯乙烯）嵌段共聚物通过复分解聚合和自由 - 自由基聚合

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Abstract >It is successfully realized that block copolymers are synthesized via metathesis polymerization followed by free‐radical polymerization. This method is performed using styrene (St) and norbornene, one block is synthesized using the Grubbs second generation catalyst in the presence of chain transfer agents, and the subsequent polymerization of St is initiated by azo compounds to complete the additional blocks in the copolymers. The use of free‐radical polymerization instead of controlled radical polymerization or ionic polymerization can be potentially superior for industrialization. As a result, the molecular weights of the block copolymers ranging from 10.4 to 54.3 kDa and polydispersity indices ranging from 1.30 to 1.91 are obtained. In principle, this new method can be potentially useful to prepare a broad range of block copolymers with cyclic olefin groups in the main chains, which may be used in some particular applications. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><abstract xmlns =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <title type =“main”>抽象</ title> >它是成功意识到嵌段共聚物通过复分解聚合，然后通过自由基聚合合成。该方法采用苯乙烯（ST）和降冰片烯进行，使用Grubbs第二代催化剂在链转移剂存在下合成一个块，并通过偶氮化合物引发ST的随后聚合以完成共聚物中的附加嵌段。使用自由基聚合代替受控的自由基聚合或离子聚合可能是工业化的可能性优势。结果，获得的嵌段共聚物的分子量为10.4至54.3kda和从1.30-1.91的范围为1.30-1.91的多分散性索引。原则上，这种新方法可能有助于制备具有主链中的环状烯烃基团的宽范围的嵌段共聚物，其可用于一些特定应用。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-33581/'>《Journal of Applied Polymer Science》</a> <b style="margin: 0 2px;">|</b><span>2018年第40期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Miao Pengcheng&option=202" target="_blank" rel="nofollow">Miao Pengcheng;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lin Shaohui&option=202" target="_blank" rel="nofollow">Lin Shaohui;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Rempel Garry L.&option=202" target="_blank" rel="nofollow">Rempel Garry L.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Pan Qinmin&option=202" target="_blank" rel="nofollow">Pan Qinmin;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Green Polymer and Catalysis Technology Laboratory College of Chemistry Chemical Engineering and Material ScienceSoochow UniversitySuzhou 215123 Jiangsu Province People's Republic of China;</p> <p>Green Polymer and Catalysis Technology Laboratory College of Chemistry Chemical Engineering and Material ScienceSoochow UniversitySuzhou 215123 Jiangsu Province People's Republic of China;</p> <p>Department of Chemical EngineeringUniversity of WaterlooWaterloo Ontario Canada;</p> <p>Green Polymer and Catalysis Technology Laboratory College of Chemistry Chemical Engineering and Material ScienceSoochow UniversitySuzhou 215123 Jiangsu Province People's Republic of China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1821.html" title="高分子化合物工业（高聚物工业）">高分子化合物工业（高聚物工业）;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=copolymers&option=203" rel="nofollow">copolymers;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=polyolefins&option=203" rel="nofollow">polyolefins;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=radical polymerization&option=203" rel="nofollow">radical polymerization;</a> </p> <div class="translation"> 机译：共聚物;聚烯烃;自由基聚合; 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tuijian_authcolor"> . 刘啸天</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘传生&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,刘传生</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=王励申&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,王励申</a> <span> <a href="/journal-cn-4590/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 东莞理工学院学报 </a> </span> <span> . 2013</span><span>,第005期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-24565_thesis/020221172349.html">原子转移自由基聚合(ATRP)合成甲氧基聚乙二醇(MPEG)-b-聚苯乙烯(Ps)嵌段共聚物的研究</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=柴月娥&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 柴月娥</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=龚福忠&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,龚福忠</a> <span> <a href="/conference-cn-24565/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 第三届全国化学工程与生物化工年会暨首届广西化学化工研究生学术论坛 </a> <span> <span> . 2006</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020312744263.html">聚（降冰片烯-聚乙交酯）-b-（降冰片烯-聚苯乙烯）二嵌段刷状共聚物的合成和性能研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=张丽秋&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 张丽秋</a> <span> . 2016</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120611355.html">降冰片烯衍生物、降冰片烯开环聚合物或共聚物以及制备该开环聚合物或共聚物的方法</a> <b>[P]</b> . <span> 中国专利： CN1787983B </span> <span> . 2010.04.28</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/061202672201.html">聚合物共混物：HDPE与乙烯‑降冰片烯或丙烯‑降冰片烯共聚物</a> <b>[P]</b> . <span> 中国专利： CN105899598B </span> <span> . 2017.11.21</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130439093770.html">Polymer modified bitumen, useful for road surfacing, comprises specific amount of block copolymer comprising triblock poly(styrene-butadiene-styrene) copolymer and diblock poly(styrene-butadiene)copolymer</a> <b>[P]</b> . <span> 外国专利： <!-- 德国专利： --> DE10330820A1 </span> <span> . 2005-02-24</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：用于道路路面的聚合物改性沥青包含特定数量的嵌段共聚物，其中包括三嵌段聚（苯乙烯-丁二烯-苯乙烯）共聚物和二嵌段聚（苯乙烯-丁二烯）共聚物 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130449971281.html">Block copolymers comprising poly benzoxazole polymer blocks and poly benzoxazinone polymer - or poly oxadiazole polymer blocks</a> <b>[P]</b> . <span> 外国专利： <!-- 德国专利： --> DE69327698T2 </span> <span> . 2000-08-17</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：包含聚苯并恶唑聚合物嵌段和聚苯并恶嗪酮聚合物嵌段共聚物或聚恶二唑聚合物嵌段的嵌段共聚物 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130435818733.html">The norbornene polymer which is the graft reaction product the macro monomer which was induced from the norbornene monomer which possesses the halogen basis which can induce the radical polymerization reaction in the end, the norbornene polymer which possesses the basis which can induce the radical polymerization reaction in the side chain, making use of that macro monomer and acrylate monomer or styrene monoma - those preparation mannered</a> <b>[P]</b> . <span> 外国专利： <!-- 日本专利： --> JP3852700B2 </span> <span> . 2006-12-06</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：接枝反应产物的降冰片烯聚合物是由具有卤素基的降冰片烯单体引发的大单体最终可以引发自由基聚合反应，具有降冰片烯聚合物的基础可以引发自由基聚合反应。侧链，利用大分子单体和丙烯酸酯单体或苯乙烯单体-那些制备方法 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704020590036','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div class="journal-sub"> <h2>期刊订阅</h2> <img src="https://cdn.zhangqiaokeyan.com/img/loginclose.png" alt="" onclick="$('.journalsub-pop-up').hide()"> <p class="pardon">抱歉，该期刊暂不可订阅，敬请期待！</p> <p 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