Bar adsorptive microextraction coated with multi-walled carbon nanotube phases - Application for trace analysis of pharmaceuticals in environmental waters

Abujaber F.; Ahmad S. M.; Neng N. R.; Rodriguez Martin-Doimeadios R. C.; Guzman Bernardo F. J.; Nogueira J. M. F.

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Bar adsorptive microextraction coated with multi-walled carbon nanotube phases - Application for trace analysis of pharmaceuticals in environmental waters

机译：具有多壁碳纳米管阶段的酒吧吸附微萃取 - 用于追踪环境水域的药物痕量分析

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Bar adsorptive microextraction devices were modified with multi-walled carbon nanotubes for the first time. A bar adsorptive microextraction method followed by microliquid desorption and high-performance liquid chromatography with diode array detection was developed for the determination of trace levels of ketoprofen, diclofenac, gemfibrozil and mefenamic acid in water samples. The mean parameters affecting the bar adsorptive microextraction and microliquid desorption efficiency were studied and optimized using a univariate optimization strategy. The methodology was validated in terms of linearity, limits of detection and quantification, recovery, intra- and inter-day precision, accuracy, and matrix effect.

机译：第一次用多壁碳纳米管改性棒状吸附微萃取装置。用于微升解吸和具有二极管阵列检测的微升沉和高效液相色谱，用于测定水样中的酮洛芬，双氯芬酸，梅花酸甲酸的微量阵列检测和高性能液相色谱法。使用单变量优化策略研究和优化影响棒状吸附微萃取和微覆盖解吸效率的平均参数。该方法在线性，检测和定量限制，恢复，日内和日常精度，准确性和矩阵效应方面进行了验证。

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《Journal of chromatography, A: Including electrophoresis and other separation methods》 |2019年第2019期|共6页
作者
Abujaber F.; Ahmad S. M.; Neng N. R.; Rodriguez Martin-Doimeadios R. C.; Guzman Bernardo F. J.; Nogueira J. M. F.;
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作者单位

Univ Castilla La Mancha Dept Analyt Chem &

Food Technol Environm Sci Inst ICAM Avda Carlos III S-N Toledo 45071 Spain;

Univ Lisbon Fac Ciencias Dept Quim &

Bioquim Ctr Quim &

Bioquim P-1749016 Lisbon Portugal;

Univ Lisbon Fac Ciencias Dept Quim &

Bioquim Ctr Quim &

Bioquim P-1749016 Lisbon Portugal;

Univ Castilla La Mancha Dept Analyt Chem &

Food Technol Environm Sci Inst ICAM Avda Carlos III S-N Toledo 45071 Spain;

Univ Castilla La Mancha Dept Analyt Chem &

Food Technol Environm Sci Inst ICAM Avda Carlos III S-N Toledo 45071 Spain;

Univ Lisbon Fac Ciencias Dept Quim &

Bioquim Ctr Quim &

Bioquim P-1749016 Lisbon Portugal;

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原文格式 PDF
正文语种 eng
中图分类分析化学;
关键词
Bar adsorptive microextraction; Carbon nanotubes; Floating sampling technology; Pharmaceuticals; Environmental water matrices; Liquid chromatography;

机译：酒吧吸附微萃取;碳纳米管;浮动采样技术;药物;环境水矩阵;液相色谱;

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1. Bar adsorptive microextraction coated with multi-walled carbon nanotube phases - Application for trace analysis of pharmaceuticals in environmental waters [J] . Abujaber F., Ahmad S. M., Neng N. R., Journal of chromatography, A: Including electrophoresis and other separation methods . 2019,第期

机译：具有多壁碳纳米管阶段的酒吧吸附微萃取 - 用于追踪环境水域的药物痕量分析
2. Comparison of the selectivity of different sorbent phases for bar adsorptive microextraction-Application to trace level analysis of fungicides in real matrices [J] . Almeida C., Nogueira J.M.F. Journal of chromatography, A: Including electrophoresis and other separation methods . 2012,第Null期

机译：条形吸附微萃取不同吸附剂相的选择性比较-实际基质中杀菌剂的痕量分析应用
3. Application of bar adsorptive microextraction to determine trace organic micro-pollutants in environmental water matrices [J] . Ahmad Samir M., Ide Alessandra H., Neng Nuno R., International journal of environmental analytical chemistry . 2017,第1a5期

机译：棒吸附微萃取法测定环境水基体中痕量有机微量污染物的应用
4. The Preparation of Carbon Nanotubes (CNTS) Solid Phase Microextraction (SPME) Probe and Application on the Analysis of Octylphenol and Nonylphenol in Water Coupled With Gas Chromatography-Mass Spectroscopy (GC-MS) [C] . Zheng Yongjie, SUN Dezhi, TIAN Jingzhi International Conference on Smart Materials and Nanotechnology in Engineering . 2012

机译：碳纳米管（CNT）固相微萃取（SPME）探针的制备及其在与气相色谱 - 质谱（GC-MS）相结合的水中辛基酚和壬基酚的分析
5. Chemical modification of multi-walled carbon nanotubes and their potential applications as new adsorbents for solid phase extraction from aqueous solutions. [D] . Abdel Salam, Mohamed. 2007

机译：多壁碳纳米管的化学改性及其作为从水溶液中固相萃取的新型吸附剂的潜在应用。
6. Bar Adsorptive Microextraction Coated with Carbon-Based Phase Mixtures for Performance-Enhancement to Monitor Selected Benzotriazoles Benzothiazoles and Benzenesulfonamides in Environmental Water Matrices [O] . Samir M. Ahmad, Bruno B.C. Calado, Mariana N. Oliveira, 2020

机译：棒吸附微萃取涂有碳的相混合物用于性能增强以监测所选苯并三唑苯并噻唑和苯磺胺酰胺在环境水基质中
7. Application of Solid Phase Microextraction Fiber Coated with Single-walled Carbon Nanotubes in the analysis of Aqueous Samples [O] . 马晓霞 2011

机译：固相微萃取纤维包覆单壁碳纳米管在水样分析中的应用
8. Fabrication and Characterization of Multi-Walled Carbon Nanotube (MWCNT) and Ni-Coated Multi-Walled Carbon Nanotube (Ni-MWCNT) Repair Patches for Carbon Fiber Reinforced Composite Systems [R] . Johnson, B., Caraccio, A., Tate, L. N., 2011

机译：碳纤维增强复合材料多壁碳纳米管（mWCNT）和Ni涂层多壁碳纳米管（Ni-mWCNT）修补补片的制备与表征

Bar adsorptive microextraction coated with multi-walled carbon nanotube phases - Application for trace analysis of pharmaceuticals in environmental waters

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