C-O bond formation via oxidative-coupling pathway in eutectic mixture of choline chloride/urea as a green solvent

Saberi Dariush; Manouchehri Neda; Niknam Khodabakhsh

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C-O bond formation via oxidative-coupling pathway in eutectic mixture of choline chloride/urea as a green solvent

机译：通过氧化偶联通路的C-O键形成胆碱/尿素的共晶混合物作为绿色溶剂

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C-O bond formation between terminal alkenes/benzyl alcohols as an arylcarboxy surrogate and carbonyl compounds in a biodegradable deep eutectic solvent (DES) based on choline chloride and urea was performed. By employment of TBAI as catalyst and TBHP as oxidant, various derivatives of carbonyl compounds were benzylated in alpha position in good to high yield at 90 degrees C. Moreover, alpha-oxybenzoylation of diethyl malonate with carboxylic acids was performed in the above-mentioned DES by employment of NaI as the catalyst and TBHP as the oxidant at 60 degrees C. (C) 2018 Elsevier B.V. All rights reserved.

机译：进行末端烯烃/苄醇与基于胆碱和尿素的可生物降解的深共晶溶剂（DES）中的芳基羧酸替代物和羰基化合物之间的C-O键。通过将TBAI作为催化剂和TBHP作为氧化剂，羰基化合物的各种衍生物在90℃的高屈服中苯并化。此外，在上述DES中进行丙二酸二乙基丙二酸亚羟基苯甲酸酯的α-羟基苯甲酰苯甲酸酯。通过在60℃的氧化剂中作为催化剂和TBHP的就业和TBHP，2018年ELSEVIER BV保留所有权利。

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来源
《Journal of Molecular Liquids》 |2019年第2019期|共8页
作者
Saberi Dariush; Manouchehri Neda; Niknam Khodabakhsh;
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作者单位

Persian Gulf Univ Coll Agr &

Nat Resources Dept Fisheries &

Aquaculture Bushehr 75169 Iran;

Persian Gulf Univ Fac Sci Dept Chem Bushehr 75169 Iran;

Persian Gulf Univ Fac Sci Dept Chem Bushehr 75169 Iran;

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原文格式 PDF
正文语种 eng
中图分类理论物理学;
关键词
Deep eutectic solvent; Choline chloride; Oxidative-coupling; alpha-Oxybenzoylation; Green solvent;

机译：深度共晶溶剂;胆碱;氧化偶联;α-氧释锰;绿色溶剂;

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1. C-O bond formation via oxidative-coupling pathway in eutectic mixture of choline chloride/urea as a green solvent [J] . Saberi Dariush, Manouchehri Neda, Niknam Khodabakhsh Journal of Molecular Liquids . 2019,第期

机译：通过氧化偶联通路的C-O键形成胆碱/尿素的共晶混合物作为绿色溶剂
2. Eutectic mixture of choline chloride/urea as a green solvent in synthesis of a coordination polymer:[Zn(O_3PCH_2CO_2)] centre dot NH_4 [J] . Ju-Hsiou Liao, Pei-Chi Wu, Yi-Hsuan Bai Inorganic Chemistry Communications . 2005,第4期

机译：氯化胆碱/脲作为绿色溶剂的共晶混合物，用于合成配位聚合物：[Zn（O_3PCH_2CO_2）]中心点NH_4
3. Ternary Deep Eutectic Solvent Behavior of Water and Urea-Choline Chloride Mixtures [J] . Smith Parker J., Arroyo Crystal B., Hernandez Felipe Lopez, The journal of physical chemistry, B. Condensed matter, materials, surfaces, interfaces & biophysical . 2019,第25期

机译：水和尿素氯化氯化物混合物的三元深度共晶溶剂行为
4. Theorical calculations on nonlinear optical properties of choline chloride- urea deep eutectic solvent [C] . E. Ferreira, J.E. Castellanos-Aguila, A. Vazquez, Conference on Nonlinear Optics and Applications . 2021

机译：胆碱氯化丙氨酸脲深对共晶溶剂的非线性光学性质的理论计算
5. Synthesis,Characterization and Molecular Dynamic Simulations of Aqueous Choline Chloride Deep Eutectic Solvents [D] . Asare, Sampson. 2018

机译：胆碱氯化胆碱水溶液深浓度溶剂的合成，表征及分子动态模拟
6. Environmentally Friendly Approach to Knoevenagel Condensation of Rhodanine in Choline Chloride: Urea Deep Eutectic Solvent and QSAR Studies on Their Antioxidant Activity [O] . Maja Molnar, Harshad Brahmbhatt, Vesna Rastija, 2018

机译：罗丹宁在氯化胆碱中Knoevenagel缩合的环保方法：尿素深共晶溶剂和QSAR研究其抗氧化活性
7. Doubly Ionic Hydrogen Bond Interactions Within the Choline Chloride - Urea Deep Eutectic Solvent [O] . Hunt, PA, Ashworth, C, Matthews, R, 2016

机译：氯化胆碱 - 尿素深共晶溶剂中的双离子氢键相互作用

C-O bond formation via oxidative-coupling pathway in eutectic mixture of choline chloride/urea as a green solvent

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