A magnetically recyclable iron oxide-supported copper oxide nanocatalyst (Fe3O4-CuO) for one-pot synthesis of S-aryl dithiocarbamates under solvent-free conditions

Aryanasab F.

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A magnetically recyclable iron oxide-supported copper oxide nanocatalyst (Fe3O4-CuO) for one-pot synthesis of S-aryl dithiocarbamates under solvent-free conditions

机译：在无溶剂条件下，磁性可回收的氧化铁支持的氧化铜氧化铜氧化铝炔丙炔（Fe3O4-CuO），其单罐合成S-芳基二硫代氨基磺酸盐

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A green, convenient and efficient procedure is reported for the synthesis of S-aryl dithiocarbamates by a simple one-pot three component Ullmann-type condensation of an amine, carbon disulfide and an aryl iodide. Magnetically separable and reusable copper oxide (Fe3O4-CuO) nanoparticles are used as a heterogeneous catalyst under base-and solvent-free conditions. Nanoparticles with an average size of 10-20 nm has been successfully prepared by a simple precipitation method in aqueous medium from readily available inexpensive starting materials. The catalyst could be easily separated from the reaction mixture by using an external magnet and recycled four times without significant loss in its activity.

机译：据报道了一种绿色，方便，有效的程序，通过简单的单壶三种组分Ullmann型缩合来合成S-芳基二硫代氨基酯，胺，二硫化碳和芳基碘化物。磁性可分离和可重复使用的氧化铜（Fe 3 O 4-CuO）纳米颗粒在基础和无溶剂条件下用作非均相催化剂。通过从容易获得的廉价原料中的水性介质中的简单沉淀法成功地制备了平均尺寸为10-20nm的纳米颗粒。催化剂可以通过使用外部磁铁容易地与反应混合物分离，并再循环四次，而不在其活性损失。

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《RSC Advances》 |2016年第38期|共7页
作者
Aryanasab F.;
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作者单位

SRI Dept Chem &

Petrochem Engn Karaj 31745139 Iran;

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正文语种 eng
中图分类化学;
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1. A magnetically recyclable iron oxide-supported copper oxide nanocatalyst (Fe3O4-CuO) for one-pot synthesis of S-aryl dithiocarbamates under solvent-free conditions [J] . Aryanasab F. RSC Advances . 2016,第38期

机译：在无溶剂条件下，磁性可回收的氧化铁支持的氧化铜氧化铜氧化铝炔丙炔（Fe3O4-CuO），其单罐合成S-芳基二硫代氨基磺酸盐
2. Application of Yttrium Iron Garnet as a Powerful and Recyclable Nanocatalyst for One-Pot Synthesis of Pyrano[2,3-c]pyrazole Derivatives under Solvent-Free Conditions [J] . Russian Journal of Organic Chemistry . 2019,第11期

机译：Yttrium Iron Garnet作为溶剂条件下吡喃[2,3-C]吡唑衍生物一锅合成的强大且可回收的纳米催化剂
3. Iron Oxide-Supported Copper Oxide Nanoparticles (Nanocat-Fe- CuO): Magnetically Recyclable Catalysts for the Synthesis of Pyrazole Derivatives, 4-Methoxyaniline, and Ullmann-type Condensation Reactions [J] . Sharad N. Shelke, Swapnil R. Bankar, Ganesh R. Mhaske ACS Sustainable Chemistry & Engineering . 2014,第7期

机译：氧化铁负载的氧化铜纳米颗粒（Nanocat-Fe-CuO）：用于合成吡唑衍生物，4-甲氧基苯胺和Ullmann型缩合反应的磁性可回收催化剂
4. Gitrate-capped superparamagnetic iron oxide (Fe3O4-CA) nanocatalyst for synthesis of pyrimidine derivative compound as antioxidative agent [C] . A H Cahyana, D Pratiwi, B Ardiansah International Symposium on Current Progress in Functional Materials . 2017

机译：用于合成嘧啶衍生物化合物作为抗氧化剂的乙酸盐 - 盖超顺磁性氧化铁（Fe3O4-CA）纳米催化剂
5. New developments toward the synthesis of heterocycles and applications in green chemistry. I. A simple and essentially one-pot synthesis of N-aminated heterocycles using phase transfer catalyst (Aliquat-336). II. Synthesis of pharmaceutically important pyrrole derivatives. III. Applications in green chemistry: Surfactant-mediated environmentally friendly cleavage of aromatic esters and trans-esterification under solvent-free neutral conditions . [D] . Patel, Nitinchandra. 2005

机译：杂环合成的新进展及其在绿色化学中的应用。 I.使用相转移催化剂（Aliquat-336）简单且基本上一锅合成N-胺化的杂环。二。药学上重要的吡咯衍生物的合成。三，在绿色化学中的应用：在无溶剂的中性条件下，表面活性剂介导的环境友好的芳族酯裂解和酯交换反应。
6. Spontaneous synthesis of gold nanoparticles on gum arabic-modified iron oxide nanoparticles as a magnetically recoverable nanocatalyst [O] . Chien-Chen Wu, Dong-Hwang Chen 2012

机译：在阿拉伯树胶改性的氧化铁纳米颗粒上自发合成金纳米颗粒作为可磁回收的纳米催化剂
7. Magnetic Nanoparticle Immobilized N-Propylsulfamic Acid as a Recyclable and Efficient Nanocatalyst for the Synthesis of 2H-indazolo2,1-bphthalazine-triones in Solvent-Free Conditions: Comparison with Sulfamic Acid [O] . Amin Rostami, Bahman Tahmasbi, Ako Yari 2013

机译：将磁性纳米粒子固定化N-丙基磺酸作为可再循环和有效的纳米催化剂，用于合成2H-吲唑的合成溶剂条件下的2H- Indazolo 2,1-B酞菁 - Triones：与氨基酸相比

A magnetically recyclable iron oxide-supported copper oxide nanocatalyst (Fe3O4-CuO) for one-pot synthesis of S-aryl dithiocarbamates under solvent-free conditions

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