Isocyanide-based three component reaction for synthesis of highly cyano substituted furan derivatives

Safaei Hamid Reza; Dehbozorgi Farbod

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Isocyanide-based three component reaction for synthesis of highly cyano substituted furan derivatives

机译：基于异氰化物的三种组分反应，用于合成高度氰基取代的呋喃衍生物

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A rapid and efficient solvent-free one-pot synthesis of novel alkyl amino aryl furan tricarbonitrile derivatives is described under catalyst-free conditions. This reaction was carried out through a three-component condensation reaction of isocyanides, 2-arylidenemalononitriles and benzoyl cyanide under solvent-free conditions. Neat conditions were established with many advantages, including high yield, environmentally friendliness, and easy and quick isolation of the products. The newly synthesized compounds were systematically characterized by IR, H-1 NMR, C-13 NMR and elemental analysis.

机译：在无催化剂条件下描述了新型烷基氨基芳基三腈衍生物的快速高效的无溶剂单罐合成。在无溶剂条件下，通过异氰酸酯，2-亚芳基甲醛和苯甲酰氰化物的三分 - 组分缩合反应进行该反应。整洁的条件是建立了许多优点，包括高产，环境友好，容易快速地隔离产品。通过IR，H-1 NMR，C-13 NMR和元素分析系统地表征了新合成的化合物。

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《RSC Advances》 |2016年第32期|共8页
作者
Safaei Hamid Reza; Dehbozorgi Farbod;
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Islamic Azad Univ Shiraz Branch Fac Sci Dept Appl Chem POB 71993-5 Shiraz Iran;

Islamic Azad Univ Shiraz Branch Fac Sci Dept Appl Chem POB 71993-5 Shiraz Iran;

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正文语种 eng
中图分类化学;
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1. Isocyanide-based three component reaction for synthesis of highly cyano substituted furan derivatives [J] . Safaei Hamid Reza, Dehbozorgi Farbod RSC Advances . 2016,第32期

机译：基于异氰化物的三种组分反应，用于合成高度氰基取代的呋喃衍生物
2. A Novel Isocyanide-Based Three-Component Reaction: Synthesis of Highly Substituted 1,6-Dihydropyrazine-2,3-dicarbonitrile Derivatives [J] . Ahmad Shaabani, Ali Maleki, Jafar Moghimi-Rad The Journal of Organic Chemistry . 2007,第16期

机译：一种新型的基于异氰酸酯的三组分反应：高度取代的1,6-二氢吡嗪-2,3-二碳腈衍生物的合成
3. A Novel Isocyanide-Based Three-Component Reaction: Synthesis of Highly Substituted 1,6-Dihydropyrazine-2,3-dicarbonitrile Derivatives [J] . Ahmad Shaabani, Ali Maleki, Jafar Moghimi-Rad The Journal of Organic Chemistry . 2007,第16期

机译：一种新型的基于异氰酸酯的三组分反应：高度取代的1,6-二氢吡嗪-2,3-二碳腈衍生物的合成
4. Ionic Liquid-Accelerated Three-Component Reaction——A Rapid One-Pot Synthesis of 3-substituted-5-arylidene-4-thi-azolidinone Derivatives [C] . 7th International Symposium on Green Chemistry in China(7th ISGCC'2005) . 2005

机译：离子液体促进的三组分反应-快速一锅法合成3-取代的5-芳基亚烷基-4-噻唑啉酮衍生物
5. (1) Reaction of iron(0) carbene complexes with hexafluorobutyne to form bis(trifluoromethylated) furans. (2) Cycloaddition reactions of vinylketene iron(0) with 1-chloroalkynes to form highly substituted chlorocatechol derivatives. [D] . Akhani, Ravish. 2009

机译：（1）铁（0）卡宾配合物与六氟丁炔反应形成双（三氟甲基化）呋喃。（2）乙烯酮铁（0）与1-氯炔烃的环加成反应，形成高度取代的氯邻苯二酚衍生物。
6. A Simple and Efficient Synthesis of Highly Substituted Indeno12-bpyrrole and Acenaphtho12-bpyrrole Derivatives by Tandem Three-Component Reactions [O] . Xiaodong Tang, Songlei Zhu, Ying Ma, 2018

机译：串联三组分反应简单高效合成高取代度茚并12-b吡咯和Ac 12-b吡咯衍生物
7. A Simple and Efficient Synthesis of Highly Substituted Indeno1,2-bpyrrole and Acenaphtho1,2-bpyrrole Derivatives by Tandem Three-Component Reactions [O] . Xiaodong Tang, Songlei Zhu, Ying Ma, 2018

机译：通过串联三分反应简单有效地合成高级取代的Indeno 1,2-B吡咯和AceNaphtho 1,2-B吡咯衍生物
8. Synthesis and Reactions of Highly Electrophilic Imines Containing the N-Cyano Group. [R] . Ramezanian, M., Padias, A. B., Saeva, F. D., 1990

机译：含氰基的高亲电子的合成及反应。

Isocyanide-based three component reaction for synthesis of highly cyano substituted furan derivatives

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