Aerobic photooxidative direct asymmetric aldol reactions of benzyl alcohols using water as the solvent

Fujiya A.; Nobuta T.; Yamaguchi E.; Tada N.; Miura T.; Itoh A.

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Aerobic photooxidative direct asymmetric aldol reactions of benzyl alcohols using water as the solvent

机译：使用水作为溶剂的有氧光光氧化直接不对称的苯甲醇的醛醇反应

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We report an aerobic photooxidative direct asymmetric aldol reaction using water as the solvent. In this reaction, primary benzyl alcohols are oxidized into benzaldehydes under an oxygen atmosphere using anthraquinone-2-sodium sulfonate monohydrate as an organo-photocatalyst. Stereoselective aldol reactions then proceed using a proline-type organocatalyst.

机译：我们报告了使用水作为溶剂的有氧光光氧基直接不对称的醛醇反应。在该反应中，使用蒽醌-2-磺酸钠一水合物作为有机光催化剂，在氧气气氛下将原发性苄醇氧化成苯甲醛。立体选择性醛醇反应然后使用脯氨酸型有机催化剂进行。

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来源
《RSC Advances》 |2015年第49期|共5页
作者
Fujiya A.; Nobuta T.; Yamaguchi E.; Tada N.; Miura T.; Itoh A.;
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作者单位

Gifu Pharmaceut Univ Gifu 5011196 Japan;

Gifu Pharmaceut Univ Gifu 5011196 Japan;

Gifu Pharmaceut Univ Gifu 5011196 Japan;

Gifu Pharmaceut Univ Gifu 5011196 Japan;

Tokyo Univ Pharm &

Life Sci Hachioji Tokyo 1920392 Japan;

Gifu Pharmaceut Univ Gifu 5011196 Japan;

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正文语种 eng
中图分类化学;
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1. Aerobic photooxidative direct asymmetric aldol reactions of benzyl alcohols using water as the solvent [J] . Fujiya A., Nobuta T., Yamaguchi E., RSC Advances . 2015,第49期

机译：使用水作为溶剂的有氧光光氧化直接不对称的苯甲醇的醛醇反应
2. One-Pot Aerobic Photooxidative Darzens Reaction from Styrene and Benzyl Alcohol via Phenacyl Iodide and Benzaldehyde by Using Iodine [J] . Omura Ryuji, Fujiya Akitoshi, Yamaguchi Eiji, Synthesis: International Journal of Methods in Synthetic Organic Chemistry . 2016,第22期

机译：碘和苯甲醛通过碘与苯乙烯和苄醇进行一锅好氧光氧化Darzens反应
3. One-Pot Aerobic Photooxidative Darzens Reaction from Styrene and Benzyl Alcohol via Phenacyl Iodide and Benzaldehyde by Using Iodine [J] . Omura Ryuji, Fujiya Akitoshi, Yamaguchi Eiji, Synthesis: International Journal of Methods in Synthetic Organic Chemistry . 2016,第22期

机译：通过使用碘的苯酰碘化物和苯甲酸苯乙烯和苯苄醇的一锅有氧光光氧化致法的反应
4. Solvent-free Aerobic Oxidation of Benzyl Alcohol by Resin Supported Noble Metal Catalysts [C] . Shaoxin Deng, Hu Wang, Tiehong Chen International Conference on Intelligent System and Applied Material . 2012

机译：通过树脂支撑贵金属催化剂无溶剂的有氧氧化苄醇
5. Strained silacycles in organic synthesis: The tandem aldol-allylatio/aldol-aldol reaction and their asymmetric variations. [D] . Wang, Xiaolun. 2005

机译：有机合成中的应变硅杂环化合物：串联的羟醛-烯丙基比/羟醛-羟醛反应及其不对称变化。
6. Catalytic asymmetric synthesis of CF3-substituted tertiary propargylic alcohols via direct aldol reaction of α-N3 amide [O] . Hidetoshi Noda, Fuyuki Amemiya, Karin Weidner, 2017

机译：α-N3酰胺的直接羟醛反应催化不对称合成CF3取代的叔炔丙醇
7. Hydrophobically directed aldol reactions: polystyrene-supported L-proline as a recyclable catalyst for direct asymmetric aldol reactions in the presence of water [O] . GRUTTADAURIA M, GIACALONE F, MOSSUTO MARCULESCU A, 2007

机译：疏水性羟醛反应：在水存在下，聚苯乙烯负载的L-脯氨酸可作为可回收的催化剂，用于直接不对称羟醛反应

Aerobic photooxidative direct asymmetric aldol reactions of benzyl alcohols using water as the solvent

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