One pot synthesis of acridine analogues from 1,2-diols as key reagents

Jagadishbabu Narasashetty; Shivashankar Kalegowda

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One pot synthesis of acridine analogues from 1,2-diols as key reagents

机译：1,2-二醇作为关键试剂的吖啶类似物的合成

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Lead tetraacetate have been demonstrated to be efficient, low cost and mild reagents for the one pot synthesis of acridine derivatives from a variety of 1,2-diols. 1,2-Diols are oxidised in situ to aldehydes, which in turn undergo reaction with dimedone and ammonium acetate to yield acridine derivatives. The attractive features of this process are mild reaction conditions, short reaction times, broad functional group tolerance, easy isolation of products and excellent yields. Thus, the current method utilises 1,2-diols instead of benzaldehydes to synthesise acridines derivatives.

机译：已经证明了铅四乙酸盐是一种高效，低成本和轻度试剂，用于来自各种1,2-二醇的吖啶衍生物的一个罐合成。 1,2-二醇原位氧化至醛，这反过来与醋酸亚胺和乙酸铵进行反应，得到吖啶衍生物。该方法的吸引力特征是温和的反应条件，反应时间短，官能团耐受性宽，易于分离产物和优异的产率。因此，目前的方法利用1,2-二醇而不是苯甲醛合成吖啶衍生物。

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《RSC Advances》 |2015年第115期|共7页
作者
Jagadishbabu Narasashetty; Shivashankar Kalegowda;
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Bangalore Univ PG Dept Chem Bangalore 560001 Karnataka India;

Bangalore Univ PG Dept Chem Bangalore 560001 Karnataka India;

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正文语种 eng
中图分类化学;
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1. One pot synthesis of acridine analogues from 1,2-diols as key reagents [J] . Jagadishbabu Narasashetty, Shivashankar Kalegowda RSC Advances . 2015,第115期

机译：1,2-二醇作为关键试剂的吖啶类似物的合成
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7. One Pot Synthesis of Acridine Analogues from 1,2-Diols as Key Reagents [O] . Jagadishbabu N., Shivashankar K. 2015

机译：以1,2-二醇为关键试剂一锅法合成吖啶类似物

One pot synthesis of acridine analogues from 1,2-diols as key reagents

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