A two-step continuous flow synthesis of amides from alcohol using a metal-free catalyst

Gu Jiajia; Fang Zheng; Liu Chengkou; Yang Zhao; Li Xin; Wei Ping; Guo Kai

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A two-step continuous flow synthesis of amides from alcohol using a metal-free catalyst

机译：使用无金属催化剂，从醇的两步连续流动合成氨基

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Metal-free oxidative amination of aromatic alcohols in the presence of TBHP provides convenient access to amides in 86-96% yield under mild reaction conditions within 15 min in a two-step continuous flow reactor system. This method avoids expensive transition metal catalysts and integrates alcohol oxidation and amide bond formation, which are usually accomplished separately, into a single operation.

机译：在TBHP存在下，无金属氧化胺化的芳族醇提供了在两步连续流动反应器系统的15分钟内在温和的反应条件下在86-96％产率下提供了方便的酰胺。该方法避免昂贵的过渡金属催化剂，并整合醇氧化和酰胺键形成，其通常分别完成，进入单一操作。

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来源
《RSC Advances》 |2015年第115期|共6页
作者
Gu Jiajia; Fang Zheng; Liu Chengkou; Yang Zhao; Li Xin; Wei Ping; Guo Kai;
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作者单位

Nanjing Tech Univ Coll Biotechnol &

Pharmaceut Engn Nanjing 211816 Jiangsu Peoples R China;

Nanjing Tech Univ Coll Pharm Nanjing 211816 Jiangsu Peoples R China;

Nanjing Tech Univ Coll Biotechnol &

Pharmaceut Engn Nanjing 211816 Jiangsu Peoples R China;

China Sch Pharmaceut Univ Coll Pharm Nanjing 210009 Jiangsu Peoples R China;

Nanjing Tech Univ Coll Biotechnol &

Pharmaceut Engn Nanjing 211816 Jiangsu Peoples R China;

Nanjing Tech Univ Coll Biotechnol &

Pharmaceut Engn Nanjing 211816 Jiangsu Peoples R China;

Nanjing Tech Univ Coll Biotechnol &

Pharmaceut Engn Nanjing 211816 Jiangsu Peoples R China;

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正文语种 eng
中图分类化学;
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1. A two-step continuous flow synthesis of amides from alcohol using a metal-free catalyst [J] . Gu Jiajia, Fang Zheng, Liu Chengkou, RSC Advances . 2015,第115期

机译：使用无金属催化剂，从醇的两步连续流动合成氨基
2. Highly practical oxidation of benzylic alcohol in continuous-flow system with metal-free catalyst [J] . Liu Chengkou, Fang Zheng, Yang Zhao, Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2015,第44期

机译：无金属催化剂在连续流系统中高度实用地氧化苄醇
3. Two-step continuous flow synthesis of amide via oxidative amidation of methylarene [J] . Shi Tingting, Zhang Zhimin, Yang Yuhang, Tetrahedron . 2020,第13期

机译：通过氧化酰胺酰胺的两步连续流动酰胺酰胺酰胺
4. Development of Continuous-flow Synthesis for Amide FungicidesUsing Heterogeneous Catalysts [C] . Zhibo Yu, Nagatoshi Koumura, Kazuhiko Sato 日本化学会春季年会 . 2020

机译：酰胺杀菌剂异质催化剂的连续流动合成的研制
5. The total synthesis of dolabelide A, and Synthesis of catalysts for the silylation of alcohols, and Invention of a bis-nucleophile for convergent synthesis of 1,3 diol natural products. [D] . Matthews, Christopher Frederick. 2001

机译：dolabelide A的全合成，醇甲硅烷基化的催化剂的合成，以及1,3二醇天然产物的聚合合成双亲核试剂。
6. Continuous-flow synthesis of primary amines: Metal-free reduction of aliphatic and aromatic nitro derivatives with trichlorosilane [O] . Riccardo Porta, Alessandra Puglisi, Giacomo Colombo, 2016

机译：伯胺的连续流合成：用三氯硅烷无金属还原脂肪族和芳香族硝基衍生物
7. Direct amide synthesis over core-shell TiO2@NiFe2O4 catalysts in a continuous flow radio frequency-heated reactor [O] . Liu Yawen, Gao Pengzhao, Cherkasov Nikolay, 2016

机译：连续流动射频加热反应器中核壳型TiO2 @ NiFe2O4催化剂上的直接酰胺合成

A two-step continuous flow synthesis of amides from alcohol using a metal-free catalyst

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