首页> 外文期刊>Cellulose Chemistry and Technology: International Journal for Physics, Chemistry and Technology of Cellulose and Lignin >APPLICATION POSSIBILITY OF ELECTROHYDRODYNAMIC TECHNIQUE FOR CELLULOSE EXTRACTION FROM BAGASSE: OPTIMIZATION USING RESPONSE SURFACE METHODOLOGY
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APPLICATION POSSIBILITY OF ELECTROHYDRODYNAMIC TECHNIQUE FOR CELLULOSE EXTRACTION FROM BAGASSE: OPTIMIZATION USING RESPONSE SURFACE METHODOLOGY

机译:纤维素萃取纤维质动力学技术的应用:使用响应面方法优化

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摘要

This study describes a promising alternative extraction process called electrohydrodynamic technique (EHD), used to extract cellulose from bagasse. The effects of EHD treatment time and heating time on cellulose extraction were investigated. The extraction conditions were then optimized using response surface methodology. The highest cellulose extraction yield was obtained when both independent variables were at their highest level (EHD: 2 h; heating: 3 h). A larger hydrodynamic size of cellulose was achieved under the optimum conditions, confirming the amorphous structure of cellulose created under the effect of EHD. Fourier-transform infrared spectroscopy was used to investigate the distribution of hydrogen bond types. The content of inter- and intra-molecular hydrogen bonds was altered when EHD was used for cellulose extraction. EHD significantly affected the composite-like structure of bagasse, which subsequently led to a higher cellulose extraction yield, and transition of crystalline to amorphous structure due to the disruption of the hydrogen bond network.
机译:该研究描述了一种有前途的替代提取过程,称为电流动力学技术(EHD),用于从甘蔗渣中提取纤维素。研究了EHD处理时间和加热时间对纤维素提取的影响。然后使用响应表面方法优化提取条件。当两个独立的变量处于最高水平时获得最高纤维素提取产率(EHD:2小时;加热:3小时)。在最佳条件下达到纤维素的较大的流体动力学大小,确认在EHD的作用下产生的纤维素的无定形结构。傅里叶变换红外光谱分析用于研究氢键类型的分布。当EHD用于纤维素萃取时,改变了分子间氢键的含量。 EHD显着影响了甘蔗渣的复合结构,随后导致更高的纤维素萃取产率,并且由于氢键网络的破坏而导致结晶与非晶结构的转变。

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