Synthesis of polyfunctionalized 1,1'-(alpha,omega-alkanediyl)bis(1,2,3,4-tetrahydropyridines)

Gibadullina Natalya N.; Latypova Dilara R.; Nugumanov Timur R.; Spirikhin Leonid V.; Dokichev Vladimir A.

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Synthesis of polyfunctionalized 1,1'-(alpha,omega-alkanediyl)bis(1,2,3,4-tetrahydropyridines)

机译：多官化1,1' - （α，Omega-链烷基硫基）双（1,2,3,4-四氢吡啶）的合成

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摘要

A one-pot reaction was developed for the synthesis of polyfunctionalized 1,1'-(alpha,omega-alkanediyl)bis(1,2,3,4-tetrahydropyridines) in 28-69% yields on the basis of a three-component reaction between 1,3-dicarbonyl compounds, aqueous 33% solution of formaldehyde, and alpha,omega-diamines.

机译：为基于三分组分，开发了一种用于合成多官能化1,1' - （α，ω-链烷基）的合成的1-1,1'（α，Omega-链烷基）的双（1,2,3,4-四氢吡啶）的产率 1,3-二羰基化合物，33％甲醛溶液和α，ω-二胺的反应。

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来源
《Chemistry of heterocyclic compounds》 |2017年第10期|共5页
作者
Gibadullina Natalya N.; Latypova Dilara R.; Nugumanov Timur R.; Spirikhin Leonid V.; Dokichev Vladimir A.;
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作者单位

Russian Acad Sci Ufa Inst Chem 71 Oktyabrya Ave Ufa 450054 Russia;

Russian Acad Sci Ufa Inst Chem 71 Oktyabrya Ave Ufa 450054 Russia;

Russian Acad Sci Ufa Inst Chem 71 Oktyabrya Ave Ufa 450054 Russia;

Russian Acad Sci Ufa Inst Chem 71 Oktyabrya Ave Ufa 450054 Russia;

Russian Acad Sci Ufa Inst Chem 71 Oktyabrya Ave Ufa 450054 Russia;

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原文格式 PDF
正文语种 eng
中图分类杂环化合物;
关键词
acetoacetic ester; acetylacetone; 1; 1 '-(alpha; omega-alkanediyl)bis(1; 2; 3; 4-tetrahydropyridines); alpha; omega-diamines; formaldehyde; multicomponent reaction;

机译：乙酰乙酰酯;乙酰丙酮;1;1' - （α;ω-链烷基噻吩基）双（1;2;3;4-四氢吡啶）;α;ω-二胺;甲醛;多组分反应;

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专利

1. Synthesis of polyfunctionalized 1,1'-(alpha,omega-alkanediyl)bis(1,2,3,4-tetrahydropyridines) [J] . Gibadullina Natalya N., Latypova Dilara R., Nugumanov Timur R., Chemistry of heterocyclic compounds . 2017,第10期

机译：多官化1,1' - （α，Omega-链烷基硫基）双（1,2,3,4-四氢吡啶）的合成
2. Synthesis of functionalized 2-vinyl-2,3- di hydro pyrroles and 3-methylene-1,2,3,4-tetrahydropyridines by palladium-catalyzed cyclization of β-enaminocarbonyl compounds with allylic bisacetates [J] . Masahiro Yoshida, Kouki Kinoshita, Kosuke Namba Organic & biomolecular chemistry . 2014,第15期

机译：钯催化烯丙基双乙酸酯催化β-烯氨基羰基化合物环化反应合成官能化的2-乙烯基-2,3-二氢吡咯和3-亚甲基-1,2,3,4-四氢吡啶
3. 1,4-bis(arylsulfonyl)-1,2,3,4-tetrahydropyridines in synthesis: Stereoselective homo- and hetero-Diels-Alder reactions [J] . Adelbrecht JC, Craig D, Fleming AJ, Synlett . 2005,第17期

机译：合成中的1,4-双（芳基磺酰基）-1,2,3,4-四氢吡啶类：立体选择性均和杂Diels-Alder反应
4. Electroabsorption spectroscopy of beta-carotene and alpha, omega-bis (1,1-dimethylheptyl)-1,3,5,7,9,11,13,15-hexadecaoctaene [C] . F.Rohlfing, D.D.C.Bradley, A.Eberhardt, Symposium M on new prospects on electronic properties of organic materials;Symposium K on fullerenes: From new molecules to new materials . 1996

机译：β-胡萝卜素和α，ω-双（1,1-二甲基庚基）-1,3,5,7,9,11,13,15-十六碳八烯的电吸收光谱
5. SYNTHESIS AND RESOLUTION OF SELECTED ALPHA,OMEGA- ALKANEDIYLBIS(1,2,3,4-TETRAHYDRO PHOSPHINOLINIUM) SALTS. THE USE OF PHOSPHORUS-31 NMR ANALYSIS TO MONITOR THE RESOLUTION. [D] . GURUSAMY, NARAYANASAMY. 1981

机译：选定的α，ω-烷二基（1,2,3,4-四氢邻苯二酚）盐的合成与拆分。使用磷31 NMR分析监测分离度。
6. Bis[(diaminomethylidene)azanium] 5-(1-oxido-1H-1,2,3,4-tetrazol-5-yl)-1H-1,2,3,4-tetrazol-1-olate [O] . Rong Fan, Ping Li, Seik Weng Ng 2015

机译：双[（二氨基亚甲基）氮杂] 5-（1-氧化物-1H-1,2,3,4-四唑-5-基）-1H-1,2,3,4-四唑-1-油酸酯
7. Polifunkcionalizált alifás és heterociklusos vegyületek új, alfa-azidoketonokból kiinduló szintézismódszereinek kifejlesztése = Development of new methodologies for the synthesis of polyfunctionalized aliphatic and heterocyclic compounds from alpha-azidoketones [O] . Patonay Tamás, Jekö József, Juhászné Tóth Éva, 2008

机译：由α-叠氮酮合成多官能脂肪族和杂环化合物的新方法的开发
8. Theoretical Prediction of the Heats of Formation, Densities and Relative Sensitivities, and/or Synthetic Approaches Toward the Synthesis of High Energy Dense Materials (HEDMs): 3,5-Dinitro-1,3,5-Oxadiazinane, Bis-Adjacent RDX, Bis-Adjacent HMX, 4,4',6,6'-Tetranitro-1,1'-Bis(N-oxide)-5,5',6,6'-4H,4'H-5,5'-Bisimidazo Oxadiazole, and the Open-Cage Derivative of CL-20. [R] . Byrd, E. F., Sabatini, J. J. 2015

机译：形成热，密度和相对灵敏度的理论预测，和/或合成高能量密集材料（HEDms）的合成方法：3,5-二硝基-1,3,5-恶二唑烷，双相邻RDX，Bis - 相邻的HmX，4,4'，6,6'-四硝基-1,1'-双（N-氧化物）-5,5'，6,6'-4H，4'H-5,5'-双咪唑恶二唑和CL-20的开笼衍生物。

Synthesis of polyfunctionalized 1,1'-(alpha,omega-alkanediyl)bis(1,2,3,4-tetrahydropyridines)

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