Formation of New Polymorphs of Acridine Using Dicarboxylic Acids as Crystallization Templates in Solution

Xuefeng Mei; Christian Wolf

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Formation of New Polymorphs of Acridine Using Dicarboxylic Acids as Crystallization Templates in Solution

机译：以二羧酸为溶液中结晶模板形成啶的新多晶型物

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Two new polymorphic structures of acridine have been prepared using terephthalic and cis,trans-mu-conic acid as templates in a supersaturated phase to affect the nucleation process and crystal growth of acridine by hydrogen-bonding and pi-pi interactions.Isothermal evaporation of a solution of acridine in ethanol afforded a single crystal structure consisting of V-shaped arrangements of dimeric acridine pi-stacks(acridine II),whereas the template-assisted crystallization approach resulted in the formation of the new polymorphs acridine VI and VII exhibiting less regular packing motifs.

机译：以对苯二甲酸和顺式，反式-μ-圆锥酸为模板，在过饱和相中制备了两个新的啶多晶型结构，以通过氢键和pi-pi相互作用影响new啶的成核过程和晶体生长。 ethanol啶在乙醇中的溶液得到由二聚crystal啶pi-stacks（ac啶II）的V形排列组成的单晶结构，而模板辅助结晶方法导致形成了新的多晶型a啶VI和VII，具有较少的规则堆积图案。

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《Crystal growth & design》 |2004年第6期|共5页
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Xuefeng Mei; Christian Wolf;
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1. Formation of New Polymorphs of Acridine Using Dicarboxylic Acids as Crystallization Templates in Solution [J] . Xuefeng Mei, Christian Wolf Crystal growth & design . 2004,第6期

机译：以二羧酸为溶液中结晶模板形成啶的新多晶型物
2. Asymmetric synthesis of aliphatic alpha-amino and gamma-hydroxy alpha-amino acids and introduction of a template for crystallization-induced asymmetric transformation [J] . Jakubec P, Berkes D, Kolarovic A, Synthesis: International Journal of Methods in Synthetic Organic Chemistry . 2006,第23期

机译：脂肪族α-氨基酸和γ-羟基α-氨基酸的不对称合成以及结晶诱导的不对称转化的模板的引入
3. Influence of low-molecular-weight dicarboxylic acids on the formation of calcium carbonate minerals in solutions with Mg~(2+) ions [J] . Mako Miyashita, Eri Yamada, Motoharu Kawano Journal of Mineralogical and Petrological Sciences . 2018,第4期

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4. FORMATION OF MESOPHASE SURFACTANT-TEMPLATED SILICA THIN FILMS FROM ACIDIC SOLUTIONS [C] . Edler, K.J., Brennan, International Zeolite Conference pt.A; 20040425-30; Cape Town(ZA) . 2004

机译：由酸性溶液形成介相表面活性剂模板的二氧化硅薄膜
5. Electrochemical reformation of levulinic acid and short-chain aliphatic acids and electrochemical polymerization of dicarboxylic acids. [D] . Li, Mingyu. 2016

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6. Syntheses and Antibiotic Evaluation of 2-{(2R4R)-4-Carboxy-2-hydroxypyrrolidin-1-ylcarbonyl}benzene-15-dicarboxylic Acids and 2-Carbamoylbenzene-15-dicarboxylic Acid Analogues [O] . Abdulrazaq Tukur, Isaac Asusheyi Bello, Neil Anthony Koorbanally, 2016

机译：2-{（（2R4R）-4-Carboxy-2-hydroxypyrrolidin-1-yl羰基}苯-15-二元羧酸和2-氨基甲酰基苯-15-二元羧酸的类似物的合成和抗生素评价
7. Hydroxyl radical-induced photochemical formation of dicarboxylic acids from unsaturated fatty acid (oleic acid) in aqueous solution [O] . Tedetti, Marc, Kawamura, Kimitaka, Narukawa, Masahiro, 2007

机译：羟基自由基诱导水溶液中不饱和脂肪酸（油酸）形成二羧酸的光化学反应
8. Thermodynamics of the Extraction of Dicarboxylic Acids from Aqueous Solutions [R] . Durrani, R. 1984

机译：从水溶液中萃取二羧酸的热力学

Formation of New Polymorphs of Acridine Using Dicarboxylic Acids as Crystallization Templates in Solution

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