Novel Sensor Based on Poly (1,2‐Diaminoanthraquinone) for Individual and Simultaneous Anodic Stripping Voltammetry of Cd        <sup >2+2+        , Pb        <sup >2+2+        , Cu        <sup >2+2+        and Hg        <sup >2+2+

Hassan Khalid Mahmoud; Gaber Seleem Elsaid; Altahan Mahmoud Fatehy; Azzem Magdi Abdel

摘要

Abstract > A novel electrochemical sensor based on glassy carbon electrode (GCE) modified by poly (1,2‐diaminoanthraquinone) (P1,2‐DAAQ) has been developed for individual and simultaneous determination of Cd 2+ , Pb 2+ , Cu 2+ and Hg 2+ using square wave anodic stripping voltammetry (SWASV). P1,2‐DAAQ was characterized by cyclic voltammetry (CV) and scan electron microscope (SEM). Several analytical parameters such as the type of electrolyte solution, polymer film thickness, metal deposition time and deposition potential were investigated and optimized. Optimal conditions were obtained by using five scan cycles for polymer synthesis and 120?seconds at ?1.6?V for metal electrodeposition in acetate buffer solution. Good linear responses to Cd 2+ , Pb 2+ , Cu 2+ and Hg 2+ in the concentration range from 0 to 120?μg/L were obtained. The limit of detections (LOD) for simultaneous determination of Cd 2+ , Pb 2+ , Cu 2+ and Hg 2+ were 0.3?μg/L, 0.58?μg/L, 1.94?μg/L and 0.26?μg/L, respectively. The developed method was also applied for their detection in real water samples for which favorable results obtained compared with those obtained using inductively coupled plasma – optical emission spectroscopy (ICP‐OES). </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> >基于聚多修饰的玻碳电极（GCE）的新型电化学传感器（1,2 -DIAMININANTRAQUINONE（P1,2-DAAQ）已开发用于个体和同时测定CD <SUP> 2 + </ sup>，Pb 2 + </ sup>，Cu 2 + </ sup >使用方波anodic剥离伏安法（SWASV），HG <Sup> 2 + </ sup>。 P1,2-DAAQ的特征在于循环伏安法（CV）和扫描电子显微镜（SEM）。研究了几种分析参数，例如电解质溶液，聚合物膜厚度，金属沉积时间和沉积电位的类型。通过使用用于聚合物合成的五个扫描循环获得最佳条件，在乙酸盐缓冲溶液中用于金属电沉积的120℃。浓度的良好线性响应CD <SUP> 2 + 2 + </ sup>，Cu 2 + </ sup>和hg 2 + </ sup>得到0至120？μg/ L的范围。用于同时测定CD 2 + / sop>，Pb 2 + </ sup>，Cu 2 + </ sup>和hg 2+的检测极限</ sup>分别为0.3Ωμg/ l，0.58Ωμg/ l，1.94ΩΩ·μg/ L和0.26ΩΩ·μg/ L.还应用于其在实际水上样品中的检测，与使用电感耦合等离子体光发射光谱（ICP-OES）获得的那些相比，得到的实际水样中的检测。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-22546/'>《Electroanalysis》</a> <b style="margin: 0 2px;">|</b><span>2018年第6期</span><b style="margin: 0 2px;">|</b><span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hassan Khalid Mahmoud&option=202" target="_blank" rel="nofollow">Hassan Khalid Mahmoud;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gaber Seleem Elsaid&option=202" target="_blank" rel="nofollow">Gaber Seleem Elsaid;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Altahan Mahmoud Fatehy&option=202" target="_blank" rel="nofollow">Altahan Mahmoud Fatehy;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Azzem Magdi Abdel&option=202" target="_blank" rel="nofollow">Azzem Magdi Abdel;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Electrochemistry Research Laboratory Physics and Mathematics Engineering Department Faculty of Electronic EngineeringMenoufia UniversityMenof 23952 Egypt;</p> <p>Central Laboratory for Environmental Quality MonitoringNational Water Research CenterEl-Qanater El-Khairia 13621 Egypt;</p> <p>Central Laboratory for Environmental Quality MonitoringNational Water Research CenterEl-Qanater El-Khairia 13621 Egypt;</p> <p>Electrochemistry Laboratory Chemistry Department Faculty of ScienceMenoufia UniversityShibin El-Kom 32511 Egypt;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/4817.html" title="电化学、电解、磁化学">电化学、电解、磁化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=modified poly (1&option=203" rel="nofollow">modified poly (1;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=2-diaminoanthraquinone) electrode&option=203" rel="nofollow">2-diaminoanthraquinone) electrode;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=anodic stripping voltammetry&option=203" rel="nofollow">anodic stripping voltammetry;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=heavy metals&option=203" rel="nofollow">heavy metals;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electrochemical sensor&option=203" rel="nofollow">electrochemical sensor;</a> </p> <div class="translation"> 机译：改性聚（1;2-二氨基醌）电极;阳极剥离伏安法;重金属;电化学传感器; 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href="/academic-journal-cn_journal-sun-yat-sen-university-natural-science-edition_thesis/0201293224071.html">用石灰和肥皂泡沫浮选处理含重金属离子废水的探讨 Ⅰ.含CO^(2+)、Pb^(2+)、Cd^(2+)、Cu^(2+)、Zn^(2+)废水</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=朱锡海&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 朱锡海</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=杨秀环&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,杨秀环</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=汪依凡&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,汪依凡</a> <span> <a href="/journal-cn-50620/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中山大学学报：自然科学版 </a> </span> <span> . 1981</span><span>,第1期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-33634_thesis/02022913857.html">南北极雪中的Zn<'2+>、Cd<'2+>、Pb<'2+>、Cu<'2+>、Sn<'4+>、Bi<'3+>离子与水汽化学</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘明星&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 刘明星</a> <span> <a href="/conference-cn-33634/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国海洋湖沼化学会第八届学术年会 </a> <span> <span> . 1998</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020315636214.html">石灰岩去除污水中Pb<'2+>、Cd<'2+>离子的研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=邢铭&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 邢铭</a> <span> . 2007</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120427786.html">用于同时检测Cu<Sup>2+</Sup>、Pb<Sup>2+</Sup>、Cd<Sup>2+</Sup>的阵列式薄膜传感器及其制备方法</a> <b>[P]</b> . <span> 中国专利： CN100434910C </span> <span> . 2008.11.19</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120105150992.html">用于同时检测Cu<Sup>2+</Sup>、Pb<Sup>2+</Sup>、Cd<Sup>2+</Sup>的阵列式薄膜传感器及其制备方法</a> <b>[P]</b> . <span> 中国专利： CN1945303A </span> <span> . 2007-04-11</span> </div> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704023174872','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div 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Novel Sensor Based on Poly (1,2‐Diaminoanthraquinone) for Individual and Simultaneous Anodic Stripping Voltammetry of Cd 2+2+ , Pb 2+2+ , Cu 2+2+ and Hg 2+2+

摘要

Novel Sensor Based on Poly (1,2‐Diaminoanthraquinone) for Individual and Simultaneous Anodic Stripping Voltammetry of Cd ^{2+2+ , Pb ^{2+2+ , Cu ^{2+2+ and Hg ²⁺²⁺}}}