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Synthesis of TiCx Powder via the Underwater Explosion of an Explosive

机译:通过爆炸性爆炸的水下爆炸合成TICX粉末

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摘要

In this study, a novel approach to the explosive synthesis of titanium carbide (TiC) is discussed. Nonstoichiometric TiCx powder was produced via the underwater explosion of a Ti powder encapsulated within a spherical explosive charge. The explosion process, bubble formation, and synthesis process were visualized using high-speed camera imaging. It was concluded that synthesis occurred within the detonation gas during the first expansion/contraction cycle of the bubble, which was accompanied by a strong emission of light. The recovered powders were studied using scanning electron microscopy and X-ray diffraction. Submicron particles were generated during the explosion. An increase in the carbon content of the starting powder resulted in an increase in the carbon content of the final product. No oxide byproducts were observed within the recovered powders.
机译:在该研究中,讨论了一种新的碳化钛(TIC)的爆炸性合成方法。 通过封装在球形爆炸电荷内的Ti粉末的水下爆炸产生非沸石TiCx粉末。 使用高速摄像头成像可视化爆炸过程,气泡形成和合成过程。 得出结论,在泡沫的第一膨胀/收缩周期期间,合成在爆炸气体中发生,伴随着强烈的光发射。 使用扫描电子显微镜和X射线衍射研究回收的粉末。 在爆炸过程中产生亚微米颗粒。 起始粉末的碳含量的增加导致最终产物的碳含量增加。 在回收的粉末中没有观察到氧化物副产物。

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