Calibration of CryojetHT and Cobra Plus Cryosystems used in X-ray diffraction studies

Dudka A. P.; Verin I. A.; Smirnova E. S.

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Calibration of CryojetHT and Cobra Plus Cryosystems used in X-ray diffraction studies

机译：X射线衍射研究中使用的CryojetHT和Cobra Plus低温系统的校准

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CryoJetHT (Oxford Instruments) and Cobra Plus (Oxford Cryosystems) cryosystems, which are used for sample cooling in X-ray diffraction experiments, have been calibrated. It is shown that the real temperature in the vicinity of the sample differs significantly (the deviation is as high as 8-10 K at low temperatures) from the temperature recorded by authorized sensors of these systems. The calibration results are confirmed by measurements of the unit-cell parameters of GdFe3(BO3)(4) single crystal in the temperature range of its phase transition. It is shown that, to determine the real temperature of a sample, one must perform an independent calibration of cryosystems rather than rely on their ratings.

机译：已对用于X射线衍射实验中样品冷却的CryoJetHT（牛津仪器公司）和Cobra Plus（牛津仪器系统）冷冻系统进行了校准。结果表明，样品附近的实际温度与这些系统的授权传感器记录的温度相差很大（低温下的偏差高达8-10 K）。校准结果通过在相变温度范围内测量GdFe3（BO3）（4）单晶的晶胞参数来确认。结果表明，要确定样品的真实温度，必须对冷冻系统进行独立校准，而不要依赖其额定值。

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《Crystallography reports》 |2016年第4期|共5页
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Dudka A. P.; Verin I. A.; Smirnova E. S.;
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Calibration of CryojetHT and Cobra Plus Cryosystems used in X-ray diffraction studies

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