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首页> 外文期刊>Crystallography reports >Porosity and structural parameters of Karelian shungites according to the data of small-angle synchrotron radiation scattering and microscopy
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Porosity and structural parameters of Karelian shungites according to the data of small-angle synchrotron radiation scattering and microscopy

机译:根据小角度同步加速器辐射散射和显微镜数据分析卡累利昂榴辉岩的孔隙度和结构参数

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摘要

The nanoporosity and structure of natural carbons has been investigated on the example of Karelian carbon-rich shungites by comparing the data of small-angle synchrotron radiation scattering and highresolution microscopy. The analysis of small-angle scattering data is based on the model of scattering spheres with lognormal size distribution. It is found that the structure of samples from the Maksovo and Zazhogino deposits subjected to high temperatures in the geological medium and (also to a lesser extent) a sample from the Shunga deposit can be described as an aggregation of polydisperse scattering spheres with lognormal size distribution; the characteristic scatterer size is determined for them. A comparison with microscopy data shows that these scatterers are mainly associated with pores, and the character of their size distribution is similar to that previously established for nanoglobules in schungites.
机译:通过比较小角度同步加速器辐射散射和高分辨率显微镜的数据,以卡累利阿富碳钨矿为例研究了天然碳的纳米孔隙度和结构。小角度散射数据的分析基于具有对数正态尺寸分布的散射球模型。已经发现,在地质介质中经受高温的马克索沃和扎佐吉诺矿床样品的结构,以及(在较小程度上)来自顺加矿床的样品,可以描述为大小分布呈对数正态分布的多分散散射球的聚集体。 ;为它们确定特征散射体大小。与显微镜数据的比较表明,这些散射体主要与孔有关,其尺寸分布特征类似于先前在钨矿中建立的纳米球。

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