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首页> 外文期刊>Crystallography reports >Experimental and theoretical investigation of the rocking curves measured for MoK (alpha) X-ray characteristic lines in the double-crystal nondispersive scheme
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Experimental and theoretical investigation of the rocking curves measured for MoK (alpha) X-ray characteristic lines in the double-crystal nondispersive scheme

机译:MoKαX射线特征线在双晶非色散方案中测得的摇摆曲线的实验和理论研究

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摘要

The rocking curves (RCs) for MoK (alpha 1) (sic) MoK (alpha 2) characteristic X-ray lines have been experimentally and theoretically studied in the nondispersive scheme of an X-ray double-crystal TPC-K diffractometer. The results of measurements and theoretical calculations of double-crystal RCs for characteristic X-rays from tubes with a molybdenum anode and different widths of slits show that a decrease in the slit width leads to an increase in the relative contribution of the MoK alpha 2-line RC in comparison with the intensity of the tails of the MoK (alpha 1)-line RC. It is shown that the second peak of the MoK alpha 2-line becomes increasingly pronounced in the tail of the MoK alpha 1-line RC with a decrease in the slit width. Two plane-parallel Si plates (input faces {110}, diffraction vector h < 220 >) were used as a monochromator crystal and a sample. The results of measuring double-crystal RCs are in good agreement with theoretical calculations.
机译:MoK(alpha 1)(sic)MoK(alpha 2)特征X射线线的摇摆曲线(RCs)已在X射线双晶TPC-K衍射仪的非分散方案中进行了实验和理论研究。从具有钼阳极且缝隙宽度不同的管得到的特征X射线的双晶RC的测量和理论计算结果表明,缝隙宽度的减小导致MoK alpha 2-的相对贡献增加。线RC与MoK(α1)线RC尾部的强度相比。结果表明,随着狭缝宽度的减小,MoK alpha 2线的第二个峰在MoK alpha 1线RC的尾部变得越来越明显。使用两个平面平行的硅板(输入面{110},衍射矢量h <220>)作为单色仪晶体和样品。双晶RC的测量结果与理论计算吻合良好。

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