Nonisothermal crystallization behavior of polylactide/polyethylene glycol/graphene oxide nanosheets composite films

摘要

Abstract > The nonisothermal crystallization (NIC) behavior of solution‐cast polylactide (PLA)/polyethylene glycol (PEG)/graphene oxide (GO) nanosheets composite (PLA/PEG/GO) films was examined at the selected cooling rate. The crystallization temperature ( <fi>T</fi> <sub>c</sub> ) of the PLA/PEG matrix improved with increasing the reinforcement of GO (0.5%‐2% w/w) at a constant cooling rate. Various conventional crystallization models, namely, Jeziorny, Ozawa, and Mo were employed to elucidate the NIC kinetics of the PLA/PEG/GO composite films. Results showed that the Mo equation was the best model to describe the NIC of the nanocomposite films. The activation energy ( <fi>E</fi> ) of crystallization was estimated by Friedman's method, and the values varied from 18 to 186?kJ·mol ?1 , however, the values were not systematic with the loading concentration of GO. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 在所选冷却速率下检查溶液浇铸聚氯酰基（PLA）/聚乙二醇（PEG）/石墨烯（GO）纳米烯氧化物（GO）纳米烯氧化物（PLA / PEG / GO）膜的非等温结晶（NIC）行为。结晶温度（ <fi> t </ fi> <sub> c </ sub> PLA / PEG基质随着在恒定的冷却速率下增加GO（0.5％-2％w / w）的增强而得到改善。使用各种常规的结晶模型，即Jeziorny，Ozawa和Mo来阐明PLA / PEG /去复合膜的NIC动力学。结果表明，Mo方程是描述纳米复合膜的NIC的最佳模型。激活能量（ <fi> e </ fi> ）通过弗里德曼的方法估计结晶，并且值从18〜186变化？KJ·Mol ？1 </ sup> 然而，这些值没有系统的加载浓度。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-29566/'>《Polymer Composites》</a> <b style="margin: 0 2px;">|</b><span>2020年第5期</span><b style="margin: 0 2px;">|</b><span>共12页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/7852.html" title="增强塑料、填充塑料">增强塑料、填充塑料;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=activation energy&option=203" rel="nofollow">activation energy;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=crystallization&option=203" rel="nofollow">crystallization;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=graphene oxide nanosheets&option=203" rel="nofollow">graphene oxide nanosheets;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mo equation&option=203" rel="nofollow">Mo equation;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=scanning electron microscopy&option=203" rel="nofollow">scanning electron microscopy;</a> </p> <div class="translation"> 机译：激活能量;结晶;石墨烯氧化物纳米晶片;Mo方程;扫描电子显微镜; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704024546649.html">Nonisothermal crystallization behavior of polylactide/polyethylene glycol/graphene oxide nanosheets composite films</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> </a> <a href="/journal-foreign-29566/" target="_blank" rel="nofollow" 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