Synthesis and structural characterization of two coordination polymers constructed by bis(4-(1H-imidazol-1-yl)phenyl) methanone and 5-(tert-butyl)isophthalate ligands

Wang Gao-Feng; Sun Shu-Wen; Wang Wei-Bing; Sun Hong; Song Shao-Fei

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Synthesis and structural characterization of two coordination polymers constructed by bis(4-(1H-imidazol-1-yl)phenyl) methanone and 5-(tert-butyl)isophthalate ligands

机译：双（4-（1H-（1H-（1H-咪唑-1-基）苯基）甲基酮和5-（叔丁基）双邻苯二甲酸酯配体构建的两种配位聚合物的合成及结构表征

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Two coordination polymers, {[Co(bipmo) (tbip)] center dot 3H(2)O}(n) (1) and {[Cd(bipmo)(tbip)] center dot 3H(2)O}(n) (2) (bipmo = bis(4-(1H-imidazol-1-yl)phenyl)methanone, H-2 tbip=5-tert-butylisophthalic acid), were synthesized by solvothermal methods and structurally characterized by elemental analyses, infrared spectroscopy, and single-crystal X-ray diffraction. The results from single-crystal X-ray diffraction data indicate that the solid state structures of 1 and 2 consist of metal-aromatic carboxylate layers, which are pillared by weak interactions to generate a three-dimensional network. The topological structures of 1 and 2 are uninodal nets based on 3-connected nodes with the Schlafli symbol of {6(3)}.

机译：两个配位聚合物，{[CO（BiPMO）（TBIP）]中心点3H（2）O}（N）（1）和{[CD（BIPMO）（TBIP）]中心点3H（2）O}（n）（2）（BIPMO =双（4-（1H-咪唑-1-基）苯基）甲基酮，H-2 TBIP = 5-叔叔丁基二甲酸）通过溶剂热方法合成，并在结构形式的特征是元素分析，红外光谱和单晶X射线衍射。单晶X射线衍射数据的结果表明，1和2的固态结构由金属 - 芳族羧酸层组成，其通过弱相互作用来产生三维网络。 1和2的拓扑结构是基于3连接的节点的单向网，其中{6（3）}的Schlafli符号。

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《Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences》 |2019年第3期|共5页
作者
Wang Gao-Feng; Sun Shu-Wen; Wang Wei-Bing; Sun Hong; Song Shao-Fei;
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Yuncheng Univ Dept Appl Chem Yuncheng 044000 Peoples R China;

Yuncheng Univ Dept Appl Chem Yuncheng 044000 Peoples R China;

Yuncheng Univ Dept Appl Chem Yuncheng 044000 Peoples R China;

Yuncheng Univ Dept Appl Chem Yuncheng 044000 Peoples R China;

Yuncheng Univ Dept Appl Chem Yuncheng 044000 Peoples R China;

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正文语种 eng
中图分类化学;
关键词
cadmium; carboxylate ligand; cobalt; imidazole; topology;

机译：镉;羧酸盐配体;钴;咪唑;拓扑;

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1. Synthesis and structural characterization of two coordination polymers constructed by bis(4-(1H-imidazol-1-yl)phenyl) methanone and 5-(tert-butyl)isophthalate ligands [J] . Wang Gao-Feng, Sun Shu-Wen, Wang Wei-Bing, Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences . 2019,第3期

机译：双（4-（1H-（1H-（1H-咪唑-1-基）苯基）甲基酮和5-（叔丁基）双邻苯二甲酸酯配体构建的两种配位聚合物的合成及结构表征
2. Structural Characterization of a Zinc(II) Bishexafluoroacetylacetonate Coordination Polymer with Bis(4-(1H-Imidazol-1-Yl)Phenyl)Methanone Ligands [J] . Wang G. -F., Sun S. -W. Journal of structural chemistry . 2018,第3期

机译：锌（II）比特氟乙酰丙酮配位聚合物与双（4-（1H-咪唑-1-基）苯基）甲基酮配体的结构表征
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5. The synthesis of a new polymeric ligand poly[5-(1,3-bis-(2'-pyridylimino)isoindolyloxy)ethylene] (PBPIIIOE) [D] . Jiang, Yi. 2000

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Synthesis and structural characterization of two coordination polymers constructed by bis(4-(1H-imidazol-1-yl)phenyl) methanone and 5-(tert-butyl)isophthalate ligands

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